(S)-1-(2,2,2-Trifluoro-acetyl)-pyrrolidine-2-carboxylic acid diphenylamide

Base Information

Chemical Name:(S)-1-(2,2,2-Trifluoro-acetyl)-pyrrolidine-2-carboxylic acid diphenylamide
CAS No.:223769-31-1
Molecular Formula:C₁₉H₁₇F₃N₂O₂
Molecular Weight:362.351
Hs Code.:

Synonyms:(S)-1-(2,2,2-Trifluoro-acetyl)-pyrrolidine-2-carboxylic acid diphenylamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-1-(2,2,2-Trifluoro-acetyl)-pyrrolidine-2-carboxylic acid diphenylamide

Chemical Property:

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Technology Process of (S)-1-(2,2,2-Trifluoro-acetyl)-pyrrolidine-2-carboxylic acid diphenylamide

There total 1 articles about (S)-1-(2,2,2-Trifluoro-acetyl)-pyrrolidine-2-carboxylic acid diphenylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 319-61-9,30163-31-6,92076-93-2,134454-19-6
(S)-1-(trifluoroacetyl)pyrrolidine-2-carboxylic acid

: 223769-31-1
(S)-1-(2,2,2-Trifluoro-acetyl)-pyrrolidine-2-carboxylic acid diphenylamide

Guidance literature:: Multi-step reaction with 2 steps

1: thionyl chloride / CH₂Cl₂ / 1 h / Ambient temperature

2: CH₂Cl₂ / 12 h / Ambient temperature

With thionyl chloride; In dichloromethane;
DOI:10.1021/jo981808t

Reference yield: 76.0%

: 223769-31-1
(S)-1-(2,2,2-Trifluoro-acetyl)-pyrrolidine-2-carboxylic acid diphenylamide

: 132139-15-2
(S)-N,N-diphenyl-2-pyrrolidinecarboxamide

Guidance literature:: With sodium tetrahydroborate; In ethanol; for 3h; Heating;
DOI:10.1021/jo981808t

Reference yield:

: 223769-31-1
(S)-1-(2,2,2-Trifluoro-acetyl)-pyrrolidine-2-carboxylic acid diphenylamide

: 223769-30-0
(S)-N,N-diphenyl-2-pyrrolidinemethanamine

Guidance literature:: Multi-step reaction with 2 steps

1: 76 percent / NaBH₄ / ethanol / 3 h / Heating

With sodium tetrahydroborate; In ethanol;
DOI:10.1021/jo981808t