dithiocarbonic acid S-[2-(3-bromo-phenyl)-4-oxo-cyclobutyl]ester O-ethyl ester

Base Information

Chemical Name:dithiocarbonic acid S-[2-(3-bromo-phenyl)-4-oxo-cyclobutyl]ester O-ethyl ester
CAS No.:1164111-62-9
Molecular Formula:C₁₃H₁₃BrO₂S₂
Molecular Weight:345.281
Hs Code.:

Synonyms:dithiocarbonic acid S-[2-(3-bromo-phenyl)-4-oxo-cyclobutyl]ester O-ethyl ester

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Chemical Property of dithiocarbonic acid S-[2-(3-bromo-phenyl)-4-oxo-cyclobutyl]ester O-ethyl ester

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Technology Process of dithiocarbonic acid S-[2-(3-bromo-phenyl)-4-oxo-cyclobutyl]ester O-ethyl ester

There total 1 articles about dithiocarbonic acid S-[2-(3-bromo-phenyl)-4-oxo-cyclobutyl]ester O-ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2039-86-3,25584-47-8
3-bromostyrene

: 140-89-6
potassium ethyl xanthogenate

: 76-02-8
trifluoroacetyl chloride

: 885267-15-2
3-(3-bromo-phenyl)-cyclobutanone

: 1164111-62-9
dithiocarbonic acid S-[2-(3-bromo-phenyl)-4-oxo-cyclobutyl]ester O-ethyl ester

Guidance literature:: 3-bromostyrene; trifluoroacetyl chloride; With zinc; In diethyl ether; at 15 ℃; for 2h; Inert atmosphere; Sonication;

With acetic acid; zinc; at 20 ℃; for 0.333333h; Inert atmosphere;

potassium ethyl xanthogenate; With 1,4-diaza-bicyclo[2.2.2]octane; In N,N-dimethyl-formamide; Inert atmosphere;
DOI:10.1021/ol9010294

Reference yield: 66.0%

: 1164111-62-9
dithiocarbonic acid S-[2-(3-bromo-phenyl)-4-oxo-cyclobutyl]ester O-ethyl ester

: 1164111-57-2
3-(4-chloro-phenyl)-2-methanesulfonyl-pent-4-enoic acid ethyl ester

: 1165776-09-9
(E)-5-[2-(3-bromo-phenyl)-4-oxo-cyclobutyl]-4-(4-chlorophenyl)-pent-2-enoic acid ethyl ester

Guidance literature:: dithiocarbonic acid S-[2-(3-bromo-phenyl)-4-oxo-cyclobutyl]ester O-ethyl ester; 3-(4-chloro-phenyl)-2-methanesulfonyl-pent-4-enoic acid ethyl ester; In 1,2-dichloro-ethane; for 0.25h; Inert atmosphere; Reflux;

With dilauryl peroxide; In 1,2-dichloro-ethane; for 15h; Inert atmosphere; Reflux;
DOI:10.1021/ol9010294