benzyl 2-acetamido-3-O-<(R)-1-(benzyloxycarbonyl)ethyl>-2-deoxy-α-D-glucopyranoside 6-(octadecyl phenyl phosphate)

Base Information

Chemical Name:benzyl 2-acetamido-3-O-<(R)-1-(benzyloxycarbonyl)ethyl>-2-deoxy-α-D-glucopyranoside 6-(octadecyl phenyl phosphate)
CAS No.:108431-14-7
Molecular Formula:C₄₉H₇₂NO₁₁P
Molecular Weight:882.085
Hs Code.:

Synonyms:benzyl 2-acetamido-3-O-<(R)-1-(benzyloxycarbonyl)ethyl>-2-deoxy-α-D-glucopyranoside 6-(octadecyl phenyl phosphate)

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Chemical Property of benzyl 2-acetamido-3-O-<(R)-1-(benzyloxycarbonyl)ethyl>-2-deoxy-α-D-glucopyranoside 6-(octadecyl phenyl phosphate)

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Technology Process of benzyl 2-acetamido-3-O-<(R)-1-(benzyloxycarbonyl)ethyl>-2-deoxy-α-D-glucopyranoside 6-(octadecyl phenyl phosphate)

There total 7 articles about benzyl 2-acetamido-3-O-<(R)-1-(benzyloxycarbonyl)ethyl>-2-deoxy-α-D-glucopyranoside 6-(octadecyl phenyl phosphate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 108431-13-6
octadecyl phenyl hydrogenphosphate

: 25605-65-6
benzyl 2-acetamido-3-O-<(R)-1-(benzyloxycarbonyl)ethyl>-2-deoxy-α-D-glucopyranoside

: 108431-14-7
benzyl 2-acetamido-3-O-<(R)-1-(benzyloxycarbonyl)ethyl>-2-deoxy-α-D-glucopyranoside 6-(octadecyl phenyl phosphate)

Guidance literature:: With TPS chloride; In pyridine; for 23h; Ambient temperature;
DOI:10.1246/bcsj.59.3207

Reference yield:

: 112-92-5
1-octadecanol

: 108431-14-7
benzyl 2-acetamido-3-O-<(R)-1-(benzyloxycarbonyl)ethyl>-2-deoxy-α-D-glucopyranoside 6-(octadecyl phenyl phosphate)

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / DCC / pyridine / 40 h / Ambient temperature

2: 72 percent / TPS chloride / pyridine / 23 h / Ambient temperature

With TPS chloride; dicyclohexyl-carbodiimide; In pyridine;
DOI:10.1246/bcsj.59.3207

Reference yield:

: 701-64-4
phosphoric acid monophenyl ester

: 108431-14-7
benzyl 2-acetamido-3-O-<(R)-1-(benzyloxycarbonyl)ethyl>-2-deoxy-α-D-glucopyranoside 6-(octadecyl phenyl phosphate)

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / DCC / pyridine / 40 h / Ambient temperature

2: 72 percent / TPS chloride / pyridine / 23 h / Ambient temperature

With TPS chloride; dicyclohexyl-carbodiimide; In pyridine;
DOI:10.1246/bcsj.59.3207