Pro-Phe-Phe-OMe

Base Information

Chemical Name:Pro-Phe-Phe-OMe
CAS No.:151345-59-4
Molecular Formula:C₂₄H₂₉N₃O₄
Molecular Weight:423.512
Hs Code.:

Synonyms:Pro-Phe-Phe-OMe

Suppliers and Price of Pro-Phe-Phe-OMe

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Pro-Phe-Phe-OMe

Chemical Property:

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Technology Process of Pro-Phe-Phe-OMe

There total 5 articles about Pro-Phe-Phe-OMe which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: 733051-45-1
(S)-2-[(S)-1-((S)-1-Methoxycarbonyl-2-phenyl-ethylcarbamoyl)-2-phenyl-ethylcarbamoyl]-pyrrolidine-1-carboxylic acid benzyl ester

: 151345-59-4
Pro-Phe-Phe-OMe

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol; for 1h; under 760 Torr;
DOI:10.1021/ol049141m

Reference yield:

: 7524-50-7
methyl (2S)-2-amino-3-phenylpropanoate hydrochloride

: 151345-59-4
Pro-Phe-Phe-OMe

Guidance literature:: Multi-step reaction with 4 steps

1: EDCI; HOBt; NMM / CH₂Cl₂ / 25 °C

2: LiOH*H₂O / tetrahydrofuran; aq. methanol / 1 h / 25 °C

3: EDCI; HOBt; NMM / CH₂Cl₂ / 12 h / 25 °C

4: 53 percent / H₂ / Pd/C / methanol / 1 h / 760 Torr

With 4-methyl-morpholine; lithium hydroxide; hydrogen; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; palladium on activated charcoal; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1021/ol049141m

Reference yield:

: 23631-72-3
N-carbobenzoxy-L-prolyl-L-phenylalanine methyl ester

: 151345-59-4
Pro-Phe-Phe-OMe

Guidance literature:: Multi-step reaction with 3 steps

1: LiOH*H₂O / tetrahydrofuran; aq. methanol / 1 h / 25 °C

2: EDCI; HOBt; NMM / CH₂Cl₂ / 12 h / 25 °C

3: 53 percent / H₂ / Pd/C / methanol / 1 h / 760 Torr

With 4-methyl-morpholine; lithium hydroxide; hydrogen; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; palladium on activated charcoal; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1021/ol049141m