[2-(o-acetanilide)palladium(1-diisopropylphosphino-2-di(t-butyl)phosphinylbenzene)(2,6-lutidine)][tetrakis(3,5-bis(trifluoromethyl)phenyl)borate]

Base Information

• Chemical Name: [2-(o-acetanilide)palladium(1-diisopropylphosphino-2-di(t-butyl)phosphinylbenzene)(2,6-lutidine)][tetrakis(3,5-bis(trifluoromethyl)phenyl)borate]
• CAS No.: 1375327-40-4
• Molecular Formula: C₂₈H₄₄NO₂P₂Pd*C₃₂H₁₂BF₂₄
• Molecular Weight: 1458.25
• Mol file: 1375327-40-4.mol

Synonyms:[2-(o-acetanilide)palladium(1-diisopropylphosphino-2-di(t-butyl)phosphinylbenzene)(2,6-lutidine)][tetrakis(3,5-bis(trifluoromethyl)phenyl)borate]

Chemical Property of [2-(o-acetanilide)palladium(1-diisopropylphosphino-2-di(t-butyl)phosphinylbenzene)(2,6-lutidine)][tetrakis(3,5-bis(trifluoromethyl)phenyl)borate]

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of [2-(o-acetanilide)palladium(1-diisopropylphosphino-2-di(t-butyl)phosphinylbenzene)(2,6-lutidine)][tetrakis(3,5-bis(trifluoromethyl)phenyl)borate]

There total 2 articles about [2-(o-acetanilide)palladium(1-diisopropylphosphino-2-di(t-butyl)phosphinylbenzene)(2,6-lutidine)][tetrakis(3,5-bis(trifluoromethyl)phenyl)borate] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

(Pd(o-C6H4NHCMe=O))2(μ-Cl)2 + iPr2C6H4POtBu2 (1375327-53-9) + sodium tetrakis[(3,5-di-trifluoromethyl)phenyl]borate (79060-88-1) → [2-(o-acetanilide)palladium(1-diisopropylphosphino-2-di(t-butyl)phosphinylbenzene)(2,6-lutidine)][tetrakis(3,5-bis(trifluoromethyl)phenyl)borate] (1375327-40-4)

Guidance literature:

In dichloromethane; at -78 - 25 ℃; for 3.5h;

Reference yield: 96.0%

[K2-(o-acetanilide)palladium(1-diisopropylphosphino-2-di(t-butyl)phosphinylbenzene) (2,6-lutidine)][hexafluoroantimonate] (1375327-38-0) + sodium tetrakis[(3,5-di-trifluoromethyl)phenyl]borate (79060-88-1) → [2-(o-acetanilide)palladium(1-diisopropylphosphino-2-di(t-butyl)phosphinylbenzene)(2,6-lutidine)][tetrakis(3,5-bis(trifluoromethyl)phenyl)borate] (1375327-40-4)

Guidance literature:

In dichloromethane; treatment of palladium compd. with borate deriv. in CH2Cl2 at room temp.;

DOI:10.1021/ja303507t

upstream raw materials:

[K₂-(o-acetanilide)palladium(1-diisopropylphosphino-2-di(t-butyl)phosphinylbenzene) (2,6-lutidine)][hexafluoroantimonate]

sodium tetrakis[(3,5-di-trifluoromethyl)phenyl]borate

iPr₂C₆H₄POtBu₂