2-methyl-5-tert-butylphenyl 2-O-benzoyl-4-O-benzyl-3-O-chloroacetyl-1-thio-α-L-rhamnopyranoside

Base Information

Chemical Name:2-methyl-5-tert-butylphenyl 2-O-benzoyl-4-O-benzyl-3-O-chloroacetyl-1-thio-α-L-rhamnopyranoside
CAS No.:1384442-65-2
Molecular Formula:C₃₃H₃₇ClO₆S
Molecular Weight:597.172
Hs Code.:

Synonyms:2-methyl-5-tert-butylphenyl 2-O-benzoyl-4-O-benzyl-3-O-chloroacetyl-1-thio-α-L-rhamnopyranoside

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Chemical Property of 2-methyl-5-tert-butylphenyl 2-O-benzoyl-4-O-benzyl-3-O-chloroacetyl-1-thio-α-L-rhamnopyranoside

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Technology Process of 2-methyl-5-tert-butylphenyl 2-O-benzoyl-4-O-benzyl-3-O-chloroacetyl-1-thio-α-L-rhamnopyranoside

There total 3 articles about 2-methyl-5-tert-butylphenyl 2-O-benzoyl-4-O-benzyl-3-O-chloroacetyl-1-thio-α-L-rhamnopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1384442-64-1
5-tert-butyl-2-methylphenyl 4-O-benzyl-2-O-benzoyl-1-thio-α-L-rhamnopyranoside

: 541-88-8
Chloroacetic anhydride

: 1384442-65-2
2-methyl-5-tert-butylphenyl 2-O-benzoyl-4-O-benzyl-3-O-chloroacetyl-1-thio-α-L-rhamnopyranoside

Guidance literature:: With dmap; triethylamine; In dichloromethane; at 0 - 20 ℃; for 2h;
DOI:10.1016/j.carres.2012.01.007

Reference yield:

: 1384442-76-5
2-methyl-5-tert-butylphenyl 2-O-acetyl-4-azido-3-O-benzyl-4,6-dideoxy-β-D-glucopyranosyl-(1->3)-2-O-benzoyl-4-O-benzyl-1-thio-α-L-rhamnopyranoside

: 1384442-65-2
2-methyl-5-tert-butylphenyl 2-O-benzoyl-4-O-benzyl-3-O-chloroacetyl-1-thio-α-L-rhamnopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: acetyl chloride / methanol; dichloromethane / 4 h / 20 °C

2: dmap; triethylamine / dichloromethane / 2 h / 0 - 20 °C

With dmap; triethylamine; acetyl chloride; In methanol; dichloromethane;
DOI:10.1016/j.carres.2012.01.007

Reference yield:

: 1384442-63-0
2-methyl-5-tert-butylphenyl 1-thio-L-rhamnopyranoside

: 1384442-65-2
2-methyl-5-tert-butylphenyl 2-O-benzoyl-4-O-benzyl-3-O-chloroacetyl-1-thio-α-L-rhamnopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1.1: camphor-10-sulfonic acid / acetonitrile / 12 h / 20 °C

1.2: 2 h / 0 - 20 °C

2.1: dmap; triethylamine / dichloromethane / 2 h / 0 - 20 °C

With dmap; camphor-10-sulfonic acid; triethylamine; In dichloromethane; acetonitrile;
DOI:10.1016/j.carres.2012.01.007