methyl 3-<<4-phenyl>thio>propanoate

Base Information

• Chemical Name: methyl 3-<<4-phenyl>thio>propanoate
• CAS No.: 131042-39-2
• Molecular Formula: C₁₄H₂₁NO₃S
• Molecular Weight: 283.392

Synonyms:methyl 3-<<4-phenyl>thio>propanoate

Chemical Property of methyl 3-<<4-phenyl>thio>propanoate

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Technology Process of methyl 3-<<4-phenyl>thio>propanoate

There total 9 articles about methyl 3-<<4-phenyl>thio>propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

oxirane (75-21-8,99932-75-9) + methyl 3-<<4-(ethylamino)phenyl>thio>propanoate (131042-44-9) → methyl 3-<<4-phenyl>thio>propanoate (131042-39-2)

Guidance literature:

In tetrahydrofuran; acetic acid; for 96h; Ambient temperature;

DOI:10.1021/jm00105a038

Reference yield: 53.0%

4-benzenethiol (131042-37-0) → methyl 3-<<4-phenyl>thio>propanoate (131042-39-2) + bis<4-phenyl> disulfide (131042-38-1)

Guidance literature:

With Methyl 3-bromopropionate; potassium carbonate; In methanol; for 0.5h; Heating;

DOI:10.1021/jm00105a038

Reference yield: 14.0%

Methyl 3-bromopropionate (3395-91-3) + 4-benzenethiol (131042-37-0) → methyl 3-<<4-phenyl>thio>propanoate (131042-39-2) + bis<4-phenyl> disulfide (131042-38-1)

Guidance literature:

With potassium carbonate; In methanol; for 0.5h; Heating;

DOI:10.1021/jm00105a038

upstream raw materials:

oxirane

methyl 3-<<4-(ethylamino)phenyl>thio>propanoate

Methyl 3-bromopropionate

4-benzenethiol

Downstream raw materials:

[4-(2-Amino-ethylsulfanyl)-phenyl]-(2-chloro-ethyl)-ethyl-amine

3-<<4-<(2-chloroethyl)ethylamino>phenyl>thio>propanoic acid

methyl 3-<<4-<(2-chloroethyl)ethylamino>phenyl>thio>propanoate

N,9-bis<<2-<<4-<(2-chloroethyl)ethylamino>phenyl>thio>ethyl>amino>acridine-4-carboxamide

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