2,3,4,6-tetra-O-acetyl-β-D-[glucose-[(13)C6]]glucopyranosyl phenethylthiohydroximate

Base Information

Chemical Name:2,3,4,6-tetra-O-acetyl-β-D-[glucose-[(13)C6]]glucopyranosyl phenethylthiohydroximate
CAS No.:1173694-41-1
Molecular Formula:C₂₃H₂₉NO₁₀S
Molecular Weight:517.484
Hs Code.:

Synonyms:2,3,4,6-tetra-O-acetyl-β-D-[glucose-[(13)C6]]glucopyranosyl phenethylthiohydroximate

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Chemical Property of 2,3,4,6-tetra-O-acetyl-β-D-[glucose-[(13)C6]]glucopyranosyl phenethylthiohydroximate

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Technology Process of 2,3,4,6-tetra-O-acetyl-β-D-[glucose-[(13)C6]]glucopyranosyl phenethylthiohydroximate

There total 1 articles about 2,3,4,6-tetra-O-acetyl-β-D-[glucose-[(13)C6]]glucopyranosyl phenethylthiohydroximate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 1173694-39-7
2,3,4,6-tetra-O-acetyl-1-thio-β-D-[(13)C6]-glucopyranose

: 92988-96-0
N-hydroxy(2-phenylethyl)-oximidoyl chloride

: 1173694-41-1
2,3,4,6-tetra-O-acetyl-β-D-[glucose-[(13)C6]]glucopyranosyl phenethylthiohydroximate

Guidance literature:: With triethylamine; In tetrahydrofuran;
DOI:10.1016/j.tet.2009.04.043

Reference yield: 83.0%

: 1173694-41-1
2,3,4,6-tetra-O-acetyl-β-D-[glucose-[(13)C6]]glucopyranosyl phenethylthiohydroximate

: 1173694-42-2
C₁₇⁽¹³⁾C₆H₂₈NO₁₃S₂^(1-)*K⁽¹⁺⁾

Guidance literature:: 2,3,4,6-tetra-O-acetyl-β-D-[glucose-[(13)C6]]glucopyranosyl phenethylthiohydroximate; With pyridine; sulfur trioxide pyridine complex; In dichloromethane; for 4h; Reflux;

With potassium hydrogencarbonate; In dichloromethane; water; for 0.5h;
DOI:10.1016/j.tet.2009.04.043