2,5-Piperazinedione,3-methoxy-6-(1-methylethyl)-,(3S-cis)-(9CI)

Base Information

Chemical Name:2,5-Piperazinedione,3-methoxy-6-(1-methylethyl)-,(3S-cis)-(9CI)
CAS No.:122170-10-9
Molecular Formula:C₈H₁₄N₂O₃
Molecular Weight:186.211
Hs Code.:
Mol file:122170-10-9.mol

Synonyms:2,5-Piperazinedione,3-methoxy-6-(1-methylethyl)-,(3S-cis)-(9CI);(3S,6S)-3-METHOXY-6-(1-METHYLETHYL)PIPERAZINE-2,5-DIONE

Suppliers and Price of 2,5-Piperazinedione,3-methoxy-6-(1-methylethyl)-,(3S-cis)-(9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of 2,5-Piperazinedione,3-methoxy-6-(1-methylethyl)-,(3S-cis)-(9CI)

Chemical Property:

PSA：74.41000
LogP:-0.21870

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2,5-Piperazinedione,3-methoxy-6-(1-methylethyl)-,(3S-cis)-(9CI)

There total 4 articles about 2,5-Piperazinedione,3-methoxy-6-(1-methylethyl)-,(3S-cis)-(9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 122092-79-9
N-tert-butoxycarbonyl-L-valyl-D,L-α-methoxyglycine methyl ester

: 122092-89-1,122170-10-9
(3RS,6S)-6-isopropyl-3-methoxy-2,5-piperazinedione

Guidance literature:: With formic acid;
DOI:10.1051/jcp/1996930575

Reference yield:

: 51803-69-1
methyl 2-((2S)-2-((tert-butoxycarbonyl)amino)-3-methylbutanamido)acetate

: 122092-89-1,122170-10-9
(3RS,6S)-6-isopropyl-3-methoxy-2,5-piperazinedione

Guidance literature:: Multi-step reaction with 2 steps

1: lithium perchlorate; sodium chloride / Electrolysis

2: formic acid / 2-methyl-propan-1-ol; toluene / Reflux

With formic acid; lithium perchlorate; sodium chloride; In 2-methyl-propan-1-ol; toluene;
DOI:10.1016/j.tetasy.2011.05.002

Reference yield:

: 122092-79-9
N-tert-butoxycarbonyl-L-valyl-D,L-α-methoxyglycine methyl ester

: 122092-89-1
(3S,6R)-3-Isopropyl-6-methoxy-piperazine-2,5-dione

: 122170-10-9
(3S,6S)-3-Isopropyl-6-methoxy-piperazine-2,5-dione

Guidance literature:: With formic acid; Yield given. Multistep reaction. Yields of byproduct given; 1.) room temperature, 2 h, 2.) isobutanol, toluene, reflux, 3 h;
DOI:10.1016/S0040-4020(01)87046-0