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Technology Process of (C5H5)Re(NO)(P(C6H5)3)P(C2H5)2H(1+)*O3SCF3(1-)={(C5H5)Re(NO)(P(C6H5)3)P(C2H5)2H}{O3SCF3}

(C5H5)Re(NO)(P(C6H5)3)P(C2H5)2H(1+)*O3SCF3(1-)={(C5H5)Re(NO)(P(C6H5)3)P(C2H5)2H}{O3SCF3}

Base Information
  • Chemical Name:(C5H5)Re(NO)(P(C6H5)3)P(C2H5)2H(1+)*O3SCF3(1-)={(C5H5)Re(NO)(P(C6H5)3)P(C2H5)2H}{O3SCF3}
  • CAS No.:113036-35-4
  • Molecular Formula:CF3O3S*C27H31NOP2Re
  • Molecular Weight:782.774
  • Hs Code.:
(C<sub>5</sub>H<sub>5</sub>)Re(NO)(P(C<sub>6</sub>H<sub>5</sub>)3)P(C<sub>2</sub>H<sub>5</sub>)2H<sup>(1+)</sup>*O<sub>3</sub>SCF<sub>3</sub><sup>(1-)</sup>={(C<sub>5</sub>H<sub>5</sub>)Re(NO)(P(C<sub>6</sub>H<sub>5</sub>)3)P(C<sub>2</sub>H<sub>5</sub>)2H}{O<sub>3</sub>SCF<sub>3</sub>}

Synonyms:(C5H5)Re(NO)(P(C6H5)3)P(C2H5)2H(1+)*O3SCF3(1-)={(C5H5)Re(NO)(P(C6H5)3)P(C2H5)2H}{O3SCF3}

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Chemical Property of (C5H5)Re(NO)(P(C6H5)3)P(C2H5)2H(1+)*O3SCF3(1-)={(C5H5)Re(NO)(P(C6H5)3)P(C2H5)2H}{O3SCF3}
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Technology Process of (C5H5)Re(NO)(P(C6H5)3)P(C2H5)2H(1+)*O3SCF3(1-)={(C5H5)Re(NO)(P(C6H5)3)P(C2H5)2H}{O3SCF3}

There total 1 articles about (C5H5)Re(NO)(P(C6H5)3)P(C2H5)2H(1+)*O3SCF3(1-)={(C5H5)Re(NO)(P(C6H5)3)P(C2H5)2H}{O3SCF3} which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

(η5-cyclopentadienyl)Re(NO)(P(C6H5)3)(CF3SO3)
92695-35-7

(η5-cyclopentadienyl)Re(NO)(P(C6H5)3)(CF3SO3)

Diethylphosphine
627-49-6

Diethylphosphine

(C<sub>5</sub>H<sub>5</sub>)Re(NO)(P(C<sub>6</sub>H<sub>5</sub>)3)P(C<sub>2</sub>H<sub>5</sub>)2H<sup>(1+)</sup>*O<sub>3</sub>SCF<sub>3</sub><sup>(1-)</sup>={(C<sub>5</sub>H<sub>5</sub>)Re(NO)(P(C<sub>6</sub>H<sub>5</sub>)3)P(C<sub>2</sub>H<sub>5</sub>)2H}{O<sub>3</sub>SCF<sub>3</sub>}
113036-35-4

(C5H5)Re(NO)(P(C6H5)3)P(C2H5)2H(1+)*O3SCF3(1-)={(C5H5)Re(NO)(P(C6H5)3)P(C2H5)2H}{O3SCF3}

Guidance literature:
In benzene; (C5H5)Re(NO)PpO3SCF3 and P(C2H5)2H stirred in benzene for 4 h; after addn. of hexane formed ppt. filtered and redissolved in CH2Cl2; after addn. of ether yellow plates formed; plates filtered and dried in vacuo at 56 ° C; elem. anal.;
DOI:10.1021/ja00216a015
upstream raw materials:

(η5-cyclopentadienyl)Re(NO)(P(C6H5)3)(CF3SO3)

Diethylphosphine

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