ethyl 2-(isopropyl(((4-methoxybenzyl)oxy)carbonyl)amino)-4,5,6,7-tetrahydrobenzo[b]thiophene-3-carboxylate

Base Information

Chemical Name:ethyl 2-(isopropyl(((4-methoxybenzyl)oxy)carbonyl)amino)-4,5,6,7-tetrahydrobenzo[b]thiophene-3-carboxylate
CAS No.:1315321-54-0
Molecular Formula:C₂₃H₂₉NO₅S
Molecular Weight:431.553
Hs Code.:

Synonyms:ethyl 2-(isopropyl(((4-methoxybenzyl)oxy)carbonyl)amino)-4,5,6,7-tetrahydrobenzo[b]thiophene-3-carboxylate

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Chemical Property of ethyl 2-(isopropyl(((4-methoxybenzyl)oxy)carbonyl)amino)-4,5,6,7-tetrahydrobenzo[b]thiophene-3-carboxylate

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Technology Process of ethyl 2-(isopropyl(((4-methoxybenzyl)oxy)carbonyl)amino)-4,5,6,7-tetrahydrobenzo[b]thiophene-3-carboxylate

There total 3 articles about ethyl 2-(isopropyl(((4-methoxybenzyl)oxy)carbonyl)amino)-4,5,6,7-tetrahydrobenzo[b]thiophene-3-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 3.0%

: 75-30-9
2-iodo-propane

: 1315321-39-1
ethyl 2-((((4-methoxybenzyl)oxy)carbonyl)amino)-4,5,6,7-tetrahydrobenzo[b]thiophene-3-carboxylate

: 1315321-53-9
C₁₅H₂₁NO₄S

: 1315321-54-0
ethyl 2-(isopropyl(((4-methoxybenzyl)oxy)carbonyl)amino)-4,5,6,7-tetrahydrobenzo[b]thiophene-3-carboxylate

Guidance literature:: With tetra-(n-butyl)ammonium iodide; caesium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 27h; Inert atmosphere;
DOI:10.1039/c0ob01156h

Reference yield:

: 824-94-2
p-methoxybenzyl chloride

: 1315321-54-0
ethyl 2-(isopropyl(((4-methoxybenzyl)oxy)carbonyl)amino)-4,5,6,7-tetrahydrobenzo[b]thiophene-3-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1.1: tetra-(n-butyl)ammonium iodide; caesium carbonate / N,N-dimethyl-formamide / 1 h

1.2: 3.5 h

2.1: tetra-(n-butyl)ammonium iodide; caesium carbonate / N,N-dimethyl-formamide / 27 h / 20 °C / Inert atmosphere

With tetra-(n-butyl)ammonium iodide; caesium carbonate; In N,N-dimethyl-formamide;
DOI:10.1039/c0ob01156h

Reference yield:

: 4506-71-2
ethyl 2-amino-4,5,6,7-tetrahydrobenzo[b]thiophene-3-carboxylate

: 1315321-53-9
C₁₅H₂₁NO₄S

: 1315321-54-0
ethyl 2-(isopropyl(((4-methoxybenzyl)oxy)carbonyl)amino)-4,5,6,7-tetrahydrobenzo[b]thiophene-3-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1.1: tetra-(n-butyl)ammonium iodide; caesium carbonate / N,N-dimethyl-formamide / 1 h

1.2: 3.5 h

2.1: tetra-(n-butyl)ammonium iodide; caesium carbonate / N,N-dimethyl-formamide / 27 h / 20 °C / Inert atmosphere

With tetra-(n-butyl)ammonium iodide; caesium carbonate; In N,N-dimethyl-formamide;
DOI:10.1039/c0ob01156h