5-(4-bromophenylaminomethyl)-2-methoxyphenyl 5-phenylisoxazole-3-carboxylate

Base Information

Chemical Name:5-(4-bromophenylaminomethyl)-2-methoxyphenyl 5-phenylisoxazole-3-carboxylate
CAS No.:1363771-28-1
Molecular Formula:C₂₄H₁₉BrN₂O₄
Molecular Weight:479.33
Hs Code.:

Synonyms:5-(4-bromophenylaminomethyl)-2-methoxyphenyl 5-phenylisoxazole-3-carboxylate

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Chemical Property of 5-(4-bromophenylaminomethyl)-2-methoxyphenyl 5-phenylisoxazole-3-carboxylate

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Technology Process of 5-(4-bromophenylaminomethyl)-2-methoxyphenyl 5-phenylisoxazole-3-carboxylate

There total 6 articles about 5-(4-bromophenylaminomethyl)-2-methoxyphenyl 5-phenylisoxazole-3-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 1363770-69-7
(E)-5-(4-bromophenyliminomethyl)-2-methoxyphenyl 5-phenylisoxazole-3-carboxylate

: 1363771-28-1
5-(4-bromophenylaminomethyl)-2-methoxyphenyl 5-phenylisoxazole-3-carboxylate

Guidance literature:: With sodium tetrahydroborate; acetic acid; In benzene; at 20 - 23 ℃;
DOI:10.1134/S1070428012010216

Reference yield:

: 14442-24-1
5-phenylisoxazole-3-carbonitrile

: 1363771-28-1
5-(4-bromophenylaminomethyl)-2-methoxyphenyl 5-phenylisoxazole-3-carboxylate

Guidance literature:: Multi-step reaction with 5 steps

1: potassium hydroxide / ethanol; water / Reflux

2: thionyl chloride / 4 h / Reflux

3: triethylamine / diethyl ether / 24 h / 20 - 23 °C

4: benzene / 1.5 h / Reflux; Dean-Stark trap

5: sodium tetrahydroborate; acetic acid / benzene / 20 - 23 °C

With sodium tetrahydroborate; thionyl chloride; acetic acid; triethylamine; potassium hydroxide; In diethyl ether; ethanol; water; benzene;
DOI:10.1134/S1070428012010216

Reference yield:

: 78189-50-1
5-phenylisoxazole-3-carboxylic acid chloride

: 1363771-28-1
5-(4-bromophenylaminomethyl)-2-methoxyphenyl 5-phenylisoxazole-3-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / diethyl ether / 24 h / 20 - 23 °C

2: benzene / 1.5 h / Reflux; Dean-Stark trap

3: sodium tetrahydroborate; acetic acid / benzene / 20 - 23 °C

With sodium tetrahydroborate; acetic acid; triethylamine; In diethyl ether; benzene;
DOI:10.1134/S1070428012010216