(R)-(4-Benzyloxy-phenyl)-((S)-3-tert-butoxycarbonylamino-2-oxo-azetidin-1-yl)-acetic acid benzyl ester

Base Information

Chemical Name:(R)-(4-Benzyloxy-phenyl)-((S)-3-tert-butoxycarbonylamino-2-oxo-azetidin-1-yl)-acetic acid benzyl ester
CAS No.:76529-92-5
Molecular Formula:C₃₀H₃₂N₂O₆
Molecular Weight:516.594
Hs Code.:

Synonyms:(R)-(4-Benzyloxy-phenyl)-((S)-3-tert-butoxycarbonylamino-2-oxo-azetidin-1-yl)-acetic acid benzyl ester

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Chemical Property of (R)-(4-Benzyloxy-phenyl)-((S)-3-tert-butoxycarbonylamino-2-oxo-azetidin-1-yl)-acetic acid benzyl ester

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Technology Process of (R)-(4-Benzyloxy-phenyl)-((S)-3-tert-butoxycarbonylamino-2-oxo-azetidin-1-yl)-acetic acid benzyl ester

There total 11 articles about (R)-(4-Benzyloxy-phenyl)-((S)-3-tert-butoxycarbonylamino-2-oxo-azetidin-1-yl)-acetic acid benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 76529-99-2
benzyl glyoxylate

: 76529-92-5
(R)-(4-Benzyloxy-phenyl)-((S)-3-tert-butoxycarbonylamino-2-oxo-azetidin-1-yl)-acetic acid benzyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: Na / methanol / 1.) rom temp., 15 h 2.) 65 deg C, 1 h

2: Na / ethane-1,2-diol / 70 °C

3: rhodium (II) acetate / benzene / 2.25 h / 80 °C

With sodium; rhodium(II) acetate; In methanol; ethylene glycol; benzene;
DOI:10.1021/jo00321a007

Reference yield:

: C₂₉H₂₆N₂O₅S

: 76529-92-5
(R)-(4-Benzyloxy-phenyl)-((S)-3-tert-butoxycarbonylamino-2-oxo-azetidin-1-yl)-acetic acid benzyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: Na / ethane-1,2-diol / 70 °C

2: rhodium (II) acetate / benzene / 2.25 h / 80 °C

With sodium; rhodium(II) acetate; In ethylene glycol; benzene;
DOI:10.1021/jo00321a007

Reference yield:

: (4-Benzyloxy-phenyl)-hydroxy-acetic acid benzyl ester

: 76529-92-5
(R)-(4-Benzyloxy-phenyl)-((S)-3-tert-butoxycarbonylamino-2-oxo-azetidin-1-yl)-acetic acid benzyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 22 percent / CrO₃ / pyridine / 5 h / Ambient temperature

2: Na / methanol / 1.) rom temp., 15 h 2.) 65 deg C, 1 h

3: Na / ethane-1,2-diol / 70 °C

4: rhodium (II) acetate / benzene / 2.25 h / 80 °C

With chromium(VI) oxide; sodium; rhodium(II) acetate; In pyridine; methanol; ethylene glycol; benzene;
DOI:10.1021/jo00321a007