4-[(1H-1,2,4-Triazol-1-yl){4-(tributylstannyl)benzyl}amino]benzonitrile

Base Information

Chemical Name:4-[(1H-1,2,4-Triazol-1-yl){4-(tributylstannyl)benzyl}amino]benzonitrile
CAS No.:1260369-16-1
Molecular Formula:C₂₈H₃₉N₅Sn
Molecular Weight:564.361
Hs Code.:

Synonyms:4-[(1H-1,2,4-Triazol-1-yl){4-(tributylstannyl)benzyl}amino]benzonitrile

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Chemical Property of 4-[(1H-1,2,4-Triazol-1-yl){4-(tributylstannyl)benzyl}amino]benzonitrile

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Technology Process of 4-[(1H-1,2,4-Triazol-1-yl){4-(tributylstannyl)benzyl}amino]benzonitrile

There total 6 articles about 4-[(1H-1,2,4-Triazol-1-yl){4-(tributylstannyl)benzyl}amino]benzonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.5%

: 155720-49-3
4-(tributylstannyl)benzyl bromide

: 148869-68-5
1-[(4-cyanophenyl)amino]-1H-1,2,4-triazole

: 1260369-16-1
4-[(1H-1,2,4-Triazol-1-yl){4-(tributylstannyl)benzyl}amino]benzonitrile

Guidance literature:: With potassium carbonate; In acetone; at 20 ℃; for 21h; Inert atmosphere;

Reference yield:

: 1194-02-1,143234-87-1
4-fluorobenzonitrile

: 1260369-16-1
4-[(1H-1,2,4-Triazol-1-yl){4-(tributylstannyl)benzyl}amino]benzonitrile

Guidance literature:: Multi-step reaction with 2 steps

1: potassium tert-butylate / dimethyl sulfoxide / 20 °C

2: potassium carbonate / acetone / 21 h / 20 °C / Inert atmosphere

With potassium tert-butylate; potassium carbonate; In dimethyl sulfoxide; acetone;

Reference yield:

: 1461-22-9
tributyltin chloride

: 1260369-16-1
4-[(1H-1,2,4-Triazol-1-yl){4-(tributylstannyl)benzyl}amino]benzonitrile

Guidance literature:: Multi-step reaction with 4 steps

1.1: n-butyllithium / hexane; tetrahydrofuran / 0.83 h / -78 °C / Inert atmosphere

1.2: 1.5 h / -78 - 20 °C / Inert atmosphere

2.1: triethylamine / dichloromethane / 0.58 h / 0 °C / Inert atmosphere

3.1: potassium bromide / N,N-dimethyl-formamide / 12 h / 20 °C / Inert atmosphere

4.1: potassium carbonate / acetone / 21 h / 20 °C / Inert atmosphere

With n-butyllithium; potassium carbonate; triethylamine; potassium bromide; In tetrahydrofuran; hexane; dichloromethane; N,N-dimethyl-formamide; acetone;