[(η5-cyclopentadienyl)Fe(1,2-bis(diphenylphosphino)ethane)(CC-ferrocenyl)]

Base Information

Chemical Name:[(η5-cyclopentadienyl)Fe(1,2-bis(diphenylphosphino)ethane)(CC-ferrocenyl)]
CAS No.:173602-87-4
Molecular Formula:C₄₃H₃₈Fe₂P₂
Molecular Weight:728.416
Hs Code.:

Synonyms:[(η5-cyclopentadienyl)Fe(1,2-bis(diphenylphosphino)ethane)(CC-ferrocenyl)]

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Chemical Property of [(η5-cyclopentadienyl)Fe(1,2-bis(diphenylphosphino)ethane)(CC-ferrocenyl)]

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Technology Process of [(η5-cyclopentadienyl)Fe(1,2-bis(diphenylphosphino)ethane)(CC-ferrocenyl)]

There total 3 articles about [(η5-cyclopentadienyl)Fe(1,2-bis(diphenylphosphino)ethane)(CC-ferrocenyl)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: [(η5-cyclopentadienyl)Fe(1,2-bis(diphenylphosphino)ethane)(=C=CH)(ferrocenyl)]PF6

: 173602-87-4
[(η5-cyclopentadienyl)Fe(1,2-bis(diphenylphosphino)ethane)(CC-ferrocenyl)]

Guidance literature:: With potassium tert-butylate; In tetrahydrofuran; byproducts: KPF6, t-BuOH; Fe complex in THF was treated with t-BuOK at room temp.; extd. (ether or CH2Cl2); elem. anal.;
DOI:10.1016/j.jorganchem.2008.09.061

Reference yield: 71.0%

: 157144-29-1
(η5-cyclopentadienyl)Fe(carbonyl)2(CC(ferrocenyl))

: 1663-45-2
1,2-bis-(diphenylphosphino)ethane

: 173602-87-4
[(η5-cyclopentadienyl)Fe(1,2-bis(diphenylphosphino)ethane)(CC-ferrocenyl)]

Guidance literature:: In acetonitrile; Irradiation (UV/VIS); N2-atmosphere; irradn. (100 W Hg-lamp, 0°C, 30 min); concg., filtering, evapn., recrystn. (CH2Cl2 / hexane); elem. anal.;
DOI:10.1021/om950525d

Reference yield: 64.0%

: 1271-47-2
ferroceneacetylene

: 55451-49-5
[1,2-bis(diphenylphosphino)ethane](η5-cyclopentadienyl)iron(II) iodide

: 173602-87-4
[(η5-cyclopentadienyl)Fe(1,2-bis(diphenylphosphino)ethane)(CC-ferrocenyl)]

Guidance literature:: With MeLi; In tetrahydrofuran; diethyl ether; N2-atmosphere; stirring (15 min); evapn., chromy. (alumina), recrystn. (CH2Cl2 / hexane);
DOI:10.1021/om950525d