3-nonyloxy-1-phenyl-1,2,3,4-tetrahydroquinoline-6-carbaldehyde N-(4-formyl)phenyl-N-phenylhydrazone

Base Information

Chemical Name:3-nonyloxy-1-phenyl-1,2,3,4-tetrahydroquinoline-6-carbaldehyde N-(4-formyl)phenyl-N-phenylhydrazone
CAS No.:1564287-78-0
Molecular Formula:C₃₈H₄₃N₃O₂
Molecular Weight:573.778
Hs Code.:

Synonyms:3-nonyloxy-1-phenyl-1,2,3,4-tetrahydroquinoline-6-carbaldehyde N-(4-formyl)phenyl-N-phenylhydrazone

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Chemical Property of 3-nonyloxy-1-phenyl-1,2,3,4-tetrahydroquinoline-6-carbaldehyde N-(4-formyl)phenyl-N-phenylhydrazone

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Technology Process of 3-nonyloxy-1-phenyl-1,2,3,4-tetrahydroquinoline-6-carbaldehyde N-(4-formyl)phenyl-N-phenylhydrazone

There total 5 articles about 3-nonyloxy-1-phenyl-1,2,3,4-tetrahydroquinoline-6-carbaldehyde N-(4-formyl)phenyl-N-phenylhydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 1564287-77-9
3-nonyloxy1-phenyl-1,2,3,4-tetrahydroquinoline-6-carbaldehyde N-phenylhydrazone

: 459-57-4
4-fluorobenzaldehyde

: 1564287-78-0
3-nonyloxy-1-phenyl-1,2,3,4-tetrahydroquinoline-6-carbaldehyde N-(4-formyl)phenyl-N-phenylhydrazone

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 90 ℃; for 3h; Inert atmosphere;
DOI:10.1016/j.dyepig.2014.01.010

Reference yield:

: 3297-78-7
acetic acid 1-phenyl-1,2,3,4-tetrahydro-quinolin-3-yl ester

: 1564287-78-0
3-nonyloxy-1-phenyl-1,2,3,4-tetrahydroquinoline-6-carbaldehyde N-(4-formyl)phenyl-N-phenylhydrazone

Guidance literature:: Multi-step reaction with 5 steps

1: trichlorophosphate

2: potassium hydroxide / methanol; water / 0.58 h / Reflux

3: potassium hydroxide; sodium sulfate / N,N-dimethyl-formamide / 60 - 65 °C

4: isopropyl alcohol / 3 h / 85 °C

5: potassium carbonate / N,N-dimethyl-formamide / 3 h / 90 °C / Inert atmosphere

With potassium carbonate; sodium sulfate; potassium hydroxide; trichlorophosphate; In methanol; water; N,N-dimethyl-formamide; isopropyl alcohol; 1: |Vilsmeier-Haack Formylation;
DOI:10.1016/j.dyepig.2014.01.010

Reference yield:

: 934420-64-1
3-acetyl-1-phenyl-1,2,3,4-tetrahydroquinoline-6-carbaldehyde

: 1564287-78-0
3-nonyloxy-1-phenyl-1,2,3,4-tetrahydroquinoline-6-carbaldehyde N-(4-formyl)phenyl-N-phenylhydrazone

Guidance literature:: Multi-step reaction with 4 steps

1: potassium hydroxide / methanol; water / 0.58 h / Reflux

2: potassium hydroxide; sodium sulfate / N,N-dimethyl-formamide / 60 - 65 °C

3: isopropyl alcohol / 3 h / 85 °C

4: potassium carbonate / N,N-dimethyl-formamide / 3 h / 90 °C / Inert atmosphere

With potassium carbonate; sodium sulfate; potassium hydroxide; In methanol; water; N,N-dimethyl-formamide; isopropyl alcohol;
DOI:10.1016/j.dyepig.2014.01.010