3-[(2-hydroxy-2-methylpropyl)thiomethyl]-4',4''-dimethoxytrityl 1-methylethyl ether

Base Information

Chemical Name:3-[(2-hydroxy-2-methylpropyl)thiomethyl]-4',4''-dimethoxytrityl 1-methylethyl ether
CAS No.:541541-02-0
Molecular Formula:C₂₉H₃₆O₄S
Molecular Weight:480.668
Hs Code.:

Synonyms:3-[(2-hydroxy-2-methylpropyl)thiomethyl]-4',4''-dimethoxytrityl 1-methylethyl ether

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Chemical Property of 3-[(2-hydroxy-2-methylpropyl)thiomethyl]-4',4''-dimethoxytrityl 1-methylethyl ether

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Technology Process of 3-[(2-hydroxy-2-methylpropyl)thiomethyl]-4',4''-dimethoxytrityl 1-methylethyl ether

There total 6 articles about 3-[(2-hydroxy-2-methylpropyl)thiomethyl]-4',4''-dimethoxytrityl 1-methylethyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 14967-17-0
1-mercapto-2-methyl-2-hydroxy-propane

: 1027419-20-0
3-[bis(4-methoxyphenyl)isopropoxymethyl]benzyl bromide

: 541541-02-0
3-[(2-hydroxy-2-methylpropyl)thiomethyl]-4',4''-dimethoxytrityl 1-methylethyl ether

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 20 ℃; for 3h;

Reference yield:

: 104-92-7
1-bromo-4-methoxy-benzene

: 541541-02-0
3-[(2-hydroxy-2-methylpropyl)thiomethyl]-4',4''-dimethoxytrityl 1-methylethyl ether

Guidance literature:: Multi-step reaction with 5 steps

1.1: magnesium / tetrahydrofuran / 1 h / 20 °C

1.2: 81 percent / tetrahydrofuran / 1 h / 0 - 20 °C

2.1: acetyl chloride / 1 h / Heating

3.1: 43.2 g / pyridine / 0 °C

4.1: 77 percent Spectr_. / N-bromosuccinimide; N,N'-azobisisobutyronitrile / CCl₄ / 0.33 h / Heating

5.1: 32 g / N-ethyldiisopropylamine / dimethylformamide / 3 h / 20 °C

With pyridine; N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); magnesium; N-ethyl-N,N-diisopropylamine; acetyl chloride; In tetrahydrofuran; tetrachloromethane; N,N-dimethyl-formamide;

Reference yield:

: 99-36-5
1-methoxycarbonyl-3-methylbenzene

: 541541-02-0
3-[(2-hydroxy-2-methylpropyl)thiomethyl]-4',4''-dimethoxytrityl 1-methylethyl ether

Guidance literature:: Multi-step reaction with 5 steps

1.1: magnesium / tetrahydrofuran / 1 h / 20 °C

1.2: 81 percent / tetrahydrofuran / 1 h / 0 - 20 °C

2.1: acetyl chloride / 1 h / Heating

3.1: 43.2 g / pyridine / 0 °C

4.1: 77 percent Spectr_. / N-bromosuccinimide; N,N'-azobisisobutyronitrile / CCl₄ / 0.33 h / Heating

5.1: 32 g / N-ethyldiisopropylamine / dimethylformamide / 3 h / 20 °C

With pyridine; N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); magnesium; N-ethyl-N,N-diisopropylamine; acetyl chloride; In tetrahydrofuran; tetrachloromethane; N,N-dimethyl-formamide;