2,3,4,6-tetra-O-acetyl-1-S-4-fluorobenzohydroximoyl-1-thio-β-D-glucopyranose

Base Information

Chemical Name:2,3,4,6-tetra-O-acetyl-1-S-4-fluorobenzohydroximoyl-1-thio-β-D-glucopyranose
CAS No.:1089209-13-1
Molecular Formula:C₂₁H₂₄FNO₁₀S
Molecular Weight:501.487
Hs Code.:

Synonyms:2,3,4,6-tetra-O-acetyl-1-S-4-fluorobenzohydroximoyl-1-thio-β-D-glucopyranose

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2,3,4,6-tetra-O-acetyl-1-S-4-fluorobenzohydroximoyl-1-thio-β-D-glucopyranose

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Technology Process of 2,3,4,6-tetra-O-acetyl-1-S-4-fluorobenzohydroximoyl-1-thio-β-D-glucopyranose

There total 1 articles about 2,3,4,6-tetra-O-acetyl-1-S-4-fluorobenzohydroximoyl-1-thio-β-D-glucopyranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 19879-84-6
tetraacetyl thioglucose

: 42202-95-9
4-fluoro-N-hydroxybenzimidoyl chloride

: 1089209-13-1
2,3,4,6-tetra-O-acetyl-1-S-4-fluorobenzohydroximoyl-1-thio-β-D-glucopyranose

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; for 1h; Inert atmosphere;
DOI:10.1016/j.bmcl.2008.08.052

Reference yield: 30.0%

: 1089209-13-1
2,3,4,6-tetra-O-acetyl-1-S-4-fluorobenzohydroximoyl-1-thio-β-D-glucopyranose

: 160617-30-1
Acetic acid (5S,7R,8R,9S,10R)-8,9-diacetoxy-7-acetoxymethyl-3-(4-fluoro-phenyl)-1,6-dioxa-4-thia-2-aza-spiro[4.5]dec-2-en-10-yl ester

Guidance literature:: With N-Bromosuccinimide; In tetrachloromethane; for 0.75h; Reflux; heat lamp illumination;
DOI:10.1016/j.bmcl.2008.08.052

Reference yield:

: 1089209-13-1
2,3,4,6-tetra-O-acetyl-1-S-4-fluorobenzohydroximoyl-1-thio-β-D-glucopyranose

: 143367-92-4
1-S-4-fluorobenzohydroximoyl-1-thio-β-D-glucopyranose

Guidance literature:: 2,3,4,6-tetra-O-acetyl-1-S-4-fluorobenzohydroximoyl-1-thio-β-D-glucopyranose; With methanol; sodium methylate; at 20 ℃; for 3h;

With Amberlite IR-120 resin (H⁺ form); In methanol; pH=5 - 6;
DOI:10.1016/j.bmc.2009.05.080