4,4’-[(9,10-dihydro-9,10[1‘,2’]-benzenoanthracene-1,4-diyl)bis(oxy)]bis[3-(trifluoromethyl)benzenamine]

Base Information

Chemical Name:4,4’-[(9,10-dihydro-9,10[1‘,2’]-benzenoanthracene-1,4-diyl)bis(oxy)]bis[3-(trifluoromethyl)benzenamine]
CAS No.:1313406-76-6
Molecular Formula:C₃₄H₂₂F₆N₂O₂
Molecular Weight:604.551
Hs Code.:

Synonyms:4,4’-[(9,10-dihydro-9,10[1‘,2’]-benzenoanthracene-1,4-diyl)bis(oxy)]bis[3-(trifluoromethyl)benzenamine]

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Chemical Property of 4,4’-[(9,10-dihydro-9,10[1‘,2’]-benzenoanthracene-1,4-diyl)bis(oxy)]bis[3-(trifluoromethyl)benzenamine]

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Technology Process of 4,4’-[(9,10-dihydro-9,10[1‘,2’]-benzenoanthracene-1,4-diyl)bis(oxy)]bis[3-(trifluoromethyl)benzenamine]

There total 6 articles about 4,4’-[(9,10-dihydro-9,10[1‘,2’]-benzenoanthracene-1,4-diyl)bis(oxy)]bis[3-(trifluoromethyl)benzenamine] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 1313406-77-7
1,4-bis(4-nitro-2-trifluoromethylphenoxy)triptycene

: 1313406-76-6
4,4’-[(9,10-dihydro-9,10[1‘,2’]-benzenoanthracene-1,4-diyl)bis(oxy)]bis[3-(trifluoromethyl)benzenamine]

Guidance literature:: With palladium 10% on activated carbon; hydrazine hydrate; In ethanol; Reflux;
DOI:10.1002/pola.24748

Reference yield:

: 5969-70-0
triptycene-1,4-diol

: 1313406-76-6
4,4’-[(9,10-dihydro-9,10[1‘,2’]-benzenoanthracene-1,4-diyl)bis(oxy)]bis[3-(trifluoromethyl)benzenamine]

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / N,N-dimethyl-formamide / 8 h / 100 °C

2: palladium 10% on activated carbon; hydrazine hydrate / ethanol / Reflux

With palladium 10% on activated carbon; potassium carbonate; hydrazine hydrate; In ethanol; N,N-dimethyl-formamide;
DOI:10.1002/pola.24748

Reference yield:

: 120-12-7
anthracene

: 1313406-76-6
4,4’-[(9,10-dihydro-9,10[1‘,2’]-benzenoanthracene-1,4-diyl)bis(oxy)]bis[3-(trifluoromethyl)benzenamine]

Guidance literature:: Multi-step reaction with 4 steps

1: toluene / 4 h / Inert atmosphere; Reflux

2: water; hydrogen bromide; acetic acid / Heating

3: potassium carbonate / N,N-dimethyl-formamide / 8 h / 100 °C

4: palladium 10% on activated carbon; hydrazine hydrate / ethanol / Reflux

With palladium 10% on activated carbon; water; hydrogen bromide; potassium carbonate; hydrazine hydrate; acetic acid; In ethanol; N,N-dimethyl-formamide; toluene; 1: Diels-Alder reaction;
DOI:10.1002/pola.24748