ammonium (4-methoxyphenyl)(3-methylbutyl)dithiophosphinate

Base Information

• Chemical Name: ammonium (4-methoxyphenyl)(3-methylbutyl)dithiophosphinate
• CAS No.: 1242723-24-5
• Molecular Formula: C₁₂H₁₉OPS₂*H₃N
• Molecular Weight: 291.419
• Mol file: 1242723-24-5.mol

Synonyms:ammonium (4-methoxyphenyl)(3-methylbutyl)dithiophosphinate

Chemical Property of ammonium (4-methoxyphenyl)(3-methylbutyl)dithiophosphinate

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of ammonium (4-methoxyphenyl)(3-methylbutyl)dithiophosphinate

There total 1 articles about ammonium (4-methoxyphenyl)(3-methylbutyl)dithiophosphinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

Lawessons reagent (19172-47-5,94367-93-8) + (3-methylbutyl)magnesium bromide (4548-78-1) → ammonium (4-methoxyphenyl)(3-methylbutyl)dithiophosphinate (1242723-24-5)

Guidance literature:

Lawessons reagent; (3-methylbutyl)magnesium bromide; In diethyl ether; Cooling with ice; Reflux; Inert atmosphere;

With sulfuric acid; water; In diethyl ether; Inert atmosphere;

With ammonia; In benzene; Cooling with ice-salt;

DOI:10.1007/s11243-010-9341-6

Reference yield: 73.0%

ammonium (4-methoxyphenyl)(3-methylbutyl)dithiophosphinate (1242723-24-5) + cadmium(II) chloride (10108-64-2) → bis-{bis-[4-methoxyphenyl(3-methylbutyl)dithiophosphinato]cadmium(II)}

Guidance literature:

In ethanol; at 20 ℃;

DOI:10.1007/s12039-015-0930-y

upstream raw materials:

Lawessons reagent

(3-methylbutyl)magnesium bromide