ethyl 3-O-benzyl-4,6-O-benzylidene-2-O-phenoxythiocarbonyl-1-thio-β-D-glucopyranoside

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Chemical Name:ethyl 3-O-benzyl-4,6-O-benzylidene-2-O-phenoxythiocarbonyl-1-thio-β-D-glucopyranoside
CAS No.:141810-61-9
Molecular Formula:C₂₉H₃₀O₆S₂
Molecular Weight:538.686
Hs Code.:

Synonyms:ethyl 3-O-benzyl-4,6-O-benzylidene-2-O-phenoxythiocarbonyl-1-thio-β-D-glucopyranoside

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Chemical Property of ethyl 3-O-benzyl-4,6-O-benzylidene-2-O-phenoxythiocarbonyl-1-thio-β-D-glucopyranoside

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Technology Process of ethyl 3-O-benzyl-4,6-O-benzylidene-2-O-phenoxythiocarbonyl-1-thio-β-D-glucopyranoside

There total 4 articles about ethyl 3-O-benzyl-4,6-O-benzylidene-2-O-phenoxythiocarbonyl-1-thio-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 141810-60-8
ethyl 3-O-benzyl-4,6-O-benzylidene-1-thio-β-D-glucopyranoside

: 1005-56-7
phenylcarbonochloridothioate

: 141810-61-9
ethyl 3-O-benzyl-4,6-O-benzylidene-2-O-phenoxythiocarbonyl-1-thio-β-D-glucopyranoside

Guidance literature:: With dmap; In acetonitrile; for 16h; Ambient temperature;
DOI:10.1016/S0040-4020(01)80165-4

Reference yield:

: 20701-61-5,56119-28-9,131564-36-8,142924-31-0,151123-92-1,141899-53-8
ethyl 4,6-O-benzylidene-1-thio-β-D-glucopyranoside

: 141810-61-9
ethyl 3-O-benzyl-4,6-O-benzylidene-2-O-phenoxythiocarbonyl-1-thio-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 1) dibutyltin oxide, 2) CsF / 1) MeOH, reflux, then RT, 4 h, 2) DMF, RT, 16 h

2: 80 percent / DMAP / acetonitrile / 16 h / Ambient temperature

With dmap; di(n-butyl)tin oxide; cesium fluoride; In acetonitrile;
DOI:10.1016/S0040-4020(01)80165-4

Reference yield:

: 100-39-0
benzyl bromide

: 141810-61-9
ethyl 3-O-benzyl-4,6-O-benzylidene-2-O-phenoxythiocarbonyl-1-thio-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 1) dibutyltin oxide, 2) CsF / 1) MeOH, reflux, then RT, 4 h, 2) DMF, RT, 16 h

2: 80 percent / DMAP / acetonitrile / 16 h / Ambient temperature

With dmap; di(n-butyl)tin oxide; cesium fluoride; In acetonitrile;
DOI:10.1016/S0040-4020(01)80165-4