(19E,27E)-N¹,N²-bis(phenyl(pyridine-2-yl)methylene)ethane-1,2-diamine

Base Information

• Chemical Name: (19E,27E)-N¹,N²-bis(phenyl(pyridine-2-yl)methylene)ethane-1,2-diamine
• CAS No.: 129372-41-4
• Molecular Formula: C₂₆H₂₂N₄
• Molecular Weight: 390.487
• Mol file: 129372-41-4.mol

Synonyms:(19E,27E)-N¹,N²-bis(phenyl(pyridine-2-yl)methylene)ethane-1,2-diamine

Chemical Property of (19E,27E)-N¹,N²-bis(phenyl(pyridine-2-yl)methylene)ethane-1,2-diamine

Chemical Property:

Purity/Quality:

Safty Information:

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• Hazard Codes: 

MSDS Files:

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Technology Process of (19E,27E)-N¹,N²-bis(phenyl(pyridine-2-yl)methylene)ethane-1,2-diamine

There total 1 articles about (19E,27E)-N¹,N²-bis(phenyl(pyridine-2-yl)methylene)ethane-1,2-diamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

phenyl(pyridin-2-yl)methanone (91-02-1) + ethylenediamine (107-15-3,85404-18-8) → (19E,27E)-N1,N2-bis(phenyl(pyridine-2-yl)methylene)ethane-1,2-diamine (129372-41-4)

Guidance literature:

With formic acid; In methanol; dichloromethane; for 12h; Reflux;

DOI:10.1002/ejoc.201700772

Reference yield: 94.0%

(19E,27E)-N1,N2-bis(phenyl(pyridine-2-yl)methylene)ethane-1,2-diamine (129372-41-4) → N,N'-bis(phenyl(pyridin-2-yl)methyl)ethane-1,2-diamine

Guidance literature:

With methanol; sodium tetrahydroborate; at 0 - 20 ℃; for 2h;

DOI:10.1002/ejoc.201700772

Reference yield:

copper(II) perchlorate hexahydrate + (19E,27E)-N1,N2-bis(phenyl(pyridine-2-yl)methylene)ethane-1,2-diamine (129372-41-4) → C26H22ClCuN4O4(1+)*ClO4(1-) (1613026-29-1,1613026-31-5)

Guidance literature:

In ethanol; Reflux;

DOI:10.1016/j.molstruc.2014.04.018

upstream raw materials:

phenyl(pyridin-2-yl)methanone

ethylenediamine

Downstream raw materials:

C₂₆H₂₂ClCuN₄O₄⁽¹⁺⁾*ClO₄^(1-)