2-[4-(3,5-dichlorophenyl)-3-ethyl-5-oxo-4,5-dihydro-1H-1,2,4-triazol-1-yl]acetohydrazide

Base Information

Chemical Name:2-[4-(3,5-dichlorophenyl)-3-ethyl-5-oxo-4,5-dihydro-1H-1,2,4-triazol-1-yl]acetohydrazide
CAS No.:1403889-29-1
Molecular Formula:C₁₂H₁₃Cl₂N₅O₂
Molecular Weight:330.174
Hs Code.:

Synonyms:2-[4-(3,5-dichlorophenyl)-3-ethyl-5-oxo-4,5-dihydro-1H-1,2,4-triazol-1-yl]acetohydrazide

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Chemical Property of 2-[4-(3,5-dichlorophenyl)-3-ethyl-5-oxo-4,5-dihydro-1H-1,2,4-triazol-1-yl]acetohydrazide

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Technology Process of 2-[4-(3,5-dichlorophenyl)-3-ethyl-5-oxo-4,5-dihydro-1H-1,2,4-triazol-1-yl]acetohydrazide

There total 2 articles about 2-[4-(3,5-dichlorophenyl)-3-ethyl-5-oxo-4,5-dihydro-1H-1,2,4-triazol-1-yl]acetohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 1403889-25-7
ethyl [4-(3,5-dichlorophenyl)-3-ethyl-5-oxo-4,5-dihydro-1H-1,2,4-triazol-1-yl]acetate

: 1403889-29-1
2-[4-(3,5-dichlorophenyl)-3-ethyl-5-oxo-4,5-dihydro-1H-1,2,4-triazol-1-yl]acetohydrazide

Guidance literature:: With hydrazine hydrate; In ethanol; at 130 ℃; for 0.166667h; Temperature; Time; Microwave irradiation; Sealed tube;
DOI:10.3184/174751912X13400138806685

Reference yield:

: 1403889-20-2
4-(3,5-dichlorophenyl)-5-ethyl-2,4-dihydro-3H-1,2,4-triazol-3-one

: 1403889-29-1
2-[4-(3,5-dichlorophenyl)-3-ethyl-5-oxo-4,5-dihydro-1H-1,2,4-triazol-1-yl]acetohydrazide

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium carbonate / acetone / 0.08 h / 90 °C / Microwave irradiation; Sealed tube

1.2: 0.17 h / 90 °C / Microwave irradiation; Sealed tube

2.1: hydrazine hydrate / ethanol / 0.17 h / 130 °C / Microwave irradiation; Sealed tube

With potassium carbonate; hydrazine hydrate; In ethanol; acetone;
DOI:10.3184/174751912X13400138806685

Reference yield: 82.0%

: 75-15-0,12122-00-8
carbon disulfide

: 1403889-29-1
2-[4-(3,5-dichlorophenyl)-3-ethyl-5-oxo-4,5-dihydro-1H-1,2,4-triazol-1-yl]acetohydrazide

: 1403889-33-7
4-(3,5-dichlorophenyl)-2-[(5-mercapto-1,3,4-oxadiazol-2-yl)methyl]-5-ethyl-2,4-dihydro-3H-1,2,4-triazol-3-one

Guidance literature:: 2-[4-(3,5-dichlorophenyl)-3-ethyl-5-oxo-4,5-dihydro-1H-1,2,4-triazol-1-yl]acetohydrazide; With potassium hydroxide; In ethanol; water; at 100 ℃; for 0.0833333h; Microwave irradiation;

carbon disulfide; In ethanol; water; at 100 ℃; for 0.166667h; Temperature; Time; Microwave irradiation;
DOI:10.3184/174751912X13400138806685