C₆₁H₉₅NO₁₂

Base Information

• Chemical Name: C₆₁H₉₅NO₁₂
• CAS No.: 1046791-73-4
• Molecular Formula: C₆₁H₉₅NO₁₂
• Molecular Weight: 1034.42
• Mol file: 1046791-73-4.mol

Synonyms:C₆₁H₉₅NO₁₂

Chemical Property of C₆₁H₉₅NO₁₂

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₆₁H₉₅NO₁₂

There total 5 articles about C₆₁H₉₅NO₁₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

C67H101NO12S (1046791-71-2) → C61H95NO12 (1046791-73-4)

Guidance literature:

With dimethyl-(methylthio)-sulphonium trifluoromethanesulphonate; In dichloromethane; at 0 ℃; for 2h; Molecular sieve;

DOI:10.1016/j.tetlet.2009.12.121

Reference yield:

C73H115NO12SSi (1046791-69-8) → C61H95NO12 (1046791-73-4)

Guidance literature:

Multi-step reaction with 2 steps

1: tetrabutyl ammonium fluoride; acetic acid / tetrahydrofuran / 3 h / 0 - 20 °C / Inert atmosphere

2: dimethyl-(methylthio)-sulphonium trifluoromethanesulphonate / dichloromethane / 2 h / 0 °C / Molecular sieve; Inert atmosphere

With tetrabutyl ammonium fluoride; acetic acid; dimethyl-(methylthio)-sulphonium trifluoromethanesulphonate; In tetrahydrofuran; dichloromethane;

DOI:10.1002/chem.201003357

Reference yield:

(2S,3R,4E)-1-O-tert-butyldimethylsilyl-2-octadecanamido-4-octadecene-1,3-diol (1215008-40-4) → C61H95NO12 (1046791-73-4)

Guidance literature:

Multi-step reaction with 4 steps

1: pyridine; dmap / 23 h / 0 - 40 °C / Inert atmosphere

2: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 5 h / 0 - 20 °C / Inert atmosphere

3: tetrabutyl ammonium fluoride; acetic acid / tetrahydrofuran / 3 h / 0 - 20 °C / Inert atmosphere

4: dimethyl-(methylthio)-sulphonium trifluoromethanesulphonate / dichloromethane / 2 h / 0 °C / Molecular sieve; Inert atmosphere

With pyridine; dmap; tetrabutyl ammonium fluoride; acetic acid; dimethyl-(methylthio)-sulphonium trifluoromethanesulphonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In tetrahydrofuran; dichloromethane;

DOI:10.1002/chem.201003357

upstream raw materials:

C₆₇H₁₀₁NO₁₂S

C₇₃H₁₁₅NO₁₂SSi

(2S,3R,4E)-1-O-tert-butyldimethylsilyl-2-octadecanamido-4-octadecene-1,3-diol

(2S,3R,4E)-1-O-tert-butyldimethylsilyl-3-O-succinoyl-2-octadecanamido-4-octadecene-1,3-diol

Downstream raw materials:

C₁₁₅H₁₅₉N₃O₃₉

C₁₀₈H₁₄₄N₂O₃₂