C₂₅H₄₀O₅SSi

Base Information

Chemical Name:C₂₅H₄₀O₅SSi
CAS No.:1293966-74-1
Molecular Formula:C₂₅H₄₀O₅SSi
Molecular Weight:480.741
Hs Code.:

C<sub>25</sub>H<sub>40</sub>O<sub>5</sub>SSi

Synonyms:C₂₅H₄₀O₅SSi

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₅H₄₀O₅SSi

Chemical Property:

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Technology Process of C₂₅H₄₀O₅SSi

There total 11 articles about C₂₅H₄₀O₅SSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1293966-73-0
C₁₉H₂₆O₅S

: 18162-48-6
tert-butyldimethylsilyl chloride

: 1293966-74-1
C₂₅H₄₀O₅SSi

Guidance literature:: With 1H-imidazole; dmap; In dichloromethane; at 20 ℃; for 12h; Inert atmosphere;
DOI:10.1021/ol2007296

Reference yield:

: 1293966-33-2
C₁₉H₂₄O₅S

: 1293966-74-1
C₂₅H₄₀O₅SSi

Guidance literature:: Multi-step reaction with 4 steps

1: samarium diiodide / tetrahydrofuran; methanol / 0.5 h / -10 °C / Inert atmosphere

2: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran / 1 h / 20 °C / Inert atmosphere

3: potassium carbonate / tetrahydrofuran; methanol / 0.5 h / 0 °C / Inert atmosphere

4: 1H-imidazole; dmap / dichloromethane / 12 h / 20 °C / Inert atmosphere

With 1H-imidazole; dmap; samarium diiodide; potassium carbonate; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; methanol; dichloromethane; 2: Mitsunobu reaction;
DOI:10.1021/ol2007296

Reference yield:

: 1293966-31-0
(4S,5S)-2,2-dimethyl-4-((S)-oxiran-2-yl)-5-vinyl-1,3-dioxolane

: 1293966-74-1
C₂₅H₄₀O₅SSi

Guidance literature:: Multi-step reaction with 7 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -20 °C / Inert atmosphere

1.2: 1 h / -20 °C / Inert atmosphere

2.1: ethylmagnesium bromide; lithium chloride / tetrahydrofuran; diethyl ether / 24 h / 20 °C / Inert atmosphere

3.1: water; calcium carbonate; methyl iodide / acetonitrile / 15 h / 40 °C / Inert atmosphere

4.1: samarium diiodide / tetrahydrofuran; methanol / 0.5 h / -10 °C / Inert atmosphere

5.1: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran / 1 h / 20 °C / Inert atmosphere

6.1: potassium carbonate / tetrahydrofuran; methanol / 0.5 h / 0 °C / Inert atmosphere

7.1: 1H-imidazole; dmap / dichloromethane / 12 h / 20 °C / Inert atmosphere

With 1H-imidazole; dmap; n-butyllithium; samarium diiodide; ethylmagnesium bromide; water; potassium carbonate; triphenylphosphine; calcium carbonate; lithium chloride; diethylazodicarboxylate; methyl iodide; In tetrahydrofuran; methanol; diethyl ether; hexane; dichloromethane; acetonitrile; 5.1: Mitsunobu reaction;
DOI:10.1021/ol2007296