7,7'-bis(benzyloxy)-3,3'-bis(hydroxymethyl)-5,5'-diisopropyl-6,6'-dimethoxy<2,2'-binaphthalene>-1,1'-diol

Base Information

Chemical Name:7,7'-bis(benzyloxy)-3,3'-bis(hydroxymethyl)-5,5'-diisopropyl-6,6'-dimethoxy<2,2'-binaphthalene>-1,1'-diol
CAS No.:124895-49-4
Molecular Formula:C₄₄H₄₆O₈
Molecular Weight:702.844
Hs Code.:

Synonyms:7,7'-bis(benzyloxy)-3,3'-bis(hydroxymethyl)-5,5'-diisopropyl-6,6'-dimethoxy<2,2'-binaphthalene>-1,1'-diol

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Chemical Property of 7,7'-bis(benzyloxy)-3,3'-bis(hydroxymethyl)-5,5'-diisopropyl-6,6'-dimethoxy<2,2'-binaphthalene>-1,1'-diol

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Technology Process of 7,7'-bis(benzyloxy)-3,3'-bis(hydroxymethyl)-5,5'-diisopropyl-6,6'-dimethoxy<2,2'-binaphthalene>-1,1'-diol

There total 2 articles about 7,7'-bis(benzyloxy)-3,3'-bis(hydroxymethyl)-5,5'-diisopropyl-6,6'-dimethoxy<2,2'-binaphthalene>-1,1'-diol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 124895-48-3
7-(benzyloxy)-3-(hydroxymethyl)-5-isopropyl-6-methoxy-1-naphthol

: 124895-49-4
7,7'-bis(benzyloxy)-3,3'-bis(hydroxymethyl)-5,5'-diisopropyl-6,6'-dimethoxy<2,2'-binaphthalene>-1,1'-diol

Guidance literature:: With di-tert-butyl peroxide; In chlorobenzene; for 9h; Heating;
DOI:10.1002/hlca.19890720221

Reference yield:

: 124895-47-2
6-(benzyloxy)-4-hydroxy-8-isopropyl-7-methoxynaphthalene-2-carboxylic acid

: 124895-49-4
7,7'-bis(benzyloxy)-3,3'-bis(hydroxymethyl)-5,5'-diisopropyl-6,6'-dimethoxy<2,2'-binaphthalene>-1,1'-diol

Guidance literature:: Multi-step reaction with 2 steps

1: 82 percent / LiAlH₄ / tetrahydrofuran / Ambient temperature

2: 83 percent / (t-Bu)2O₂ / chlorobenzene / 9 h / Heating

With lithium aluminium tetrahydride; di-tert-butyl peroxide; In tetrahydrofuran; chlorobenzene;
DOI:10.1002/hlca.19890720221

Reference yield:

: 124895-49-4
7,7'-bis(benzyloxy)-3,3'-bis(hydroxymethyl)-5,5'-diisopropyl-6,6'-dimethoxy<2,2'-binaphthalene>-1,1'-diol

: 124895-50-7
3,10-bis(benzyloxy)-1,8-diisopropyl-2,9-dimethoxy-6H,13H-5,12-dioxadibenzopyrene

Guidance literature:: With phosphorus tribromide; potassium carbonate; Yield given. Multistep reaction; 1.) THF, 20 deg C, 1 h, 2) acetone, reflux, 2 h;
DOI:10.1002/hlca.19890720221