3-[2-(2-{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}ethoxy)ethoxy]-2-methylbenzyl chloride

Base Information

Chemical Name:3-[2-(2-{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}ethoxy)ethoxy]-2-methylbenzyl chloride
CAS No.:467252-60-4
Molecular Formula:C₁₉H₃₁ClO₆
Molecular Weight:390.905
Hs Code.:

Synonyms:3-[2-(2-{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}ethoxy)ethoxy]-2-methylbenzyl chloride

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Chemical Property of 3-[2-(2-{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}ethoxy)ethoxy]-2-methylbenzyl chloride

Chemical Property:

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Technology Process of 3-[2-(2-{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}ethoxy)ethoxy]-2-methylbenzyl chloride

There total 4 articles about 3-[2-(2-{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}ethoxy)ethoxy]-2-methylbenzyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 467252-58-0
3-[2-(2-{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}ethoxy)ethoxy]-2-methylbenzyl alcohol

: 467252-60-4
3-[2-(2-{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}ethoxy)ethoxy]-2-methylbenzyl chloride

Guidance literature:: With thionyl chloride; In dichloromethane; at 20 ℃; for 0.5h;
DOI:10.1021/jm0208673

Reference yield:

: 55289-05-9
methyl 3-hydroxy-2-methylbenzoate

: 467252-60-4
3-[2-(2-{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}ethoxy)ethoxy]-2-methylbenzyl chloride

Guidance literature:: Multi-step reaction with 3 steps

1: 97 percent / K₂CO₃ / acetonitrile / Heating

2: 49 percent / LiAlH₄ / tetrahydrofuran / 2 h / Heating

3: SOCl₂ / CH₂Cl₂ / 0.5 h / 20 °C

With lithium aluminium tetrahydride; thionyl chloride; potassium carbonate; In tetrahydrofuran; dichloromethane; acetonitrile;
DOI:10.1021/jm0208673

Reference yield:

: 130955-38-3
2,5,8,11,14-pentaoxahexadecan-16-yl methanesulfonate

: 467252-60-4
3-[2-(2-{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}ethoxy)ethoxy]-2-methylbenzyl chloride

Guidance literature:: Multi-step reaction with 3 steps

1: 97 percent / K₂CO₃ / acetonitrile / Heating

2: 49 percent / LiAlH₄ / tetrahydrofuran / 2 h / Heating

3: SOCl₂ / CH₂Cl₂ / 0.5 h / 20 °C

With lithium aluminium tetrahydride; thionyl chloride; potassium carbonate; In tetrahydrofuran; dichloromethane; acetonitrile;
DOI:10.1021/jm0208673