2-Acetylamino-3-(2-acetylamino-2-benzyloxycarbonyl-ethylsulfanyl)-propionic acid benzyl ester

Base Information

Chemical Name:2-Acetylamino-3-(2-acetylamino-2-benzyloxycarbonyl-ethylsulfanyl)-propionic acid benzyl ester
CAS No.:73908-44-8
Molecular Formula:C₂₄H₂₈N₂O₆S
Molecular Weight:472.562
Hs Code.:

Synonyms:2-Acetylamino-3-(2-acetylamino-2-benzyloxycarbonyl-ethylsulfanyl)-propionic acid benzyl ester

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Chemical Property of 2-Acetylamino-3-(2-acetylamino-2-benzyloxycarbonyl-ethylsulfanyl)-propionic acid benzyl ester

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Technology Process of 2-Acetylamino-3-(2-acetylamino-2-benzyloxycarbonyl-ethylsulfanyl)-propionic acid benzyl ester

There total 4 articles about 2-Acetylamino-3-(2-acetylamino-2-benzyloxycarbonyl-ethylsulfanyl)-propionic acid benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 73908-42-6
N-acetyl-L-cysteine benzylester

: 73908-43-7
2-acetylamino-acrylic acid benzyl ester

: 73908-44-8
2-Acetylamino-3-(2-acetylamino-2-benzyloxycarbonyl-ethylsulfanyl)-propionic acid benzyl ester

: 73908-45-9
(R)-2-Acetylamino-3-(2-acetylamino-2-benzyloxycarbonyl-ethylsulfanyl)-propionic acid benzyl ester

Guidance literature:: With N-cyclohexyl-N'-β-(4-methylmorpholinium)ethylcarbodiimide p-toluenesulfonate; copper(l) chloride; In dichloromethane; at 20 ℃; for 12h; Yield given;
DOI:10.1021/jo01303a043

Reference yield:

: 73908-42-6
N-acetyl-L-cysteine benzylester

: 73908-44-8
2-Acetylamino-3-(2-acetylamino-2-benzyloxycarbonyl-ethylsulfanyl)-propionic acid benzyl ester

: 73908-45-9
(R)-2-Acetylamino-3-(2-acetylamino-2-benzyloxycarbonyl-ethylsulfanyl)-propionic acid benzyl ester

Guidance literature:: With diisopropyl-carbodiimide; In acetonitrile; at 20 ℃; for 5h; Yield given. Title compound not separated from byproducts;
DOI:10.1021/jo01303a043

Reference yield:

: 2978-10-1
O-benzyl-N,N'-diisopropylisourea

: 73908-44-8
2-Acetylamino-3-(2-acetylamino-2-benzyloxycarbonyl-ethylsulfanyl)-propionic acid benzyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 44 percent

2: 1-cyclohexyl-3-(2-morpholinoethyl)-carbodiimide metho-p-toluenesulfonate / CH₂Cl₂ / 12 h / 20 °C

With N-cyclohexyl-N'-β-(4-methylmorpholinium)ethylcarbodiimide p-toluenesulfonate; In dichloromethane;
DOI:10.1021/jo01303a043