Technology Process of C27H32F2N4O13
There total 5 articles about C27H32F2N4O13 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: acetic acid; zinc / 1 h / 20 °C
2.1: acetic acid; sodium nitrite / water / 2 h / 0 °C
2.2: 0.5 h / 0 - 20 °C
3.1: 36 h / 20 °C / Inert atmosphere; Neat (no solvent)
3.2: 24 h / 20 °C / Inert atmosphere
4.1: diethylamino-sulfur trifluoride / dichloromethane / 3 h / 20 °C / Inert atmosphere
With
diethylamino-sulfur trifluoride; acetic acid; zinc; sodium nitrite;
In
dichloromethane; water;
DOI:10.1016/j.bmc.2012.02.001
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: 36 h / 20 °C / Inert atmosphere; Neat (no solvent)
1.2: 24 h / 20 °C / Inert atmosphere
2.1: diethylamino-sulfur trifluoride / dichloromethane / 3 h / 20 °C / Inert atmosphere
With
diethylamino-sulfur trifluoride;
In
dichloromethane;
DOI:10.1016/j.bmc.2012.02.001
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: acetic acid; sodium nitrite / water / 2 h / 0 °C
1.2: 0.5 h / 0 - 20 °C
2.1: 36 h / 20 °C / Inert atmosphere; Neat (no solvent)
2.2: 24 h / 20 °C / Inert atmosphere
3.1: diethylamino-sulfur trifluoride / dichloromethane / 3 h / 20 °C / Inert atmosphere
With
diethylamino-sulfur trifluoride; acetic acid; sodium nitrite;
In
dichloromethane; water;
DOI:10.1016/j.bmc.2012.02.001
