2-(4-CF₃-C₆H₄-NCH)C₄H₃NH

Base Information

Chemical Name:2-(4-CF₃-C₆H₄-NCH)C₄H₃NH
CAS No.:274687-50-2
Molecular Formula:C₁₂H₉F₃N₂
Molecular Weight:238.212
Hs Code.:

2-(4-CF<sub>3</sub>-C<sub>6</sub>H<sub>4</sub>-NCH)C<sub>4</sub>H<sub>3</sub>NH

Synonyms:2-(4-CF₃-C₆H₄-NCH)C₄H₃NH

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Chemical Property of 2-(4-CF₃-C₆H₄-NCH)C₄H₃NH

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Technology Process of 2-(4-CF₃-C₆H₄-NCH)C₄H₃NH

There total 1 articles about 2-(4-CF₃-C₆H₄-NCH)C₄H₃NH which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1003-29-8,254729-95-8
2-pyrrole aldehyde

: 455-14-1
4-trifluoromethylphenylamine

: 274687-50-2
2-(4-CF₃-C₆H₄-NCH)C₄H₃NH

Guidance literature:: With formic acid; In ethanol; at 20 ℃; for 48h;
DOI:10.1039/b909495d

Reference yield: 83.0%

: 274687-50-2
2-(4-CF₃-C₆H₄-NCH)C₄H₃NH

: 75-24-1
trimethylaluminum

: [2-(4-(CF₃)C₆H₄N=CH)C₄H₃N]2AlCH₃

Guidance literature:: In dichloromethane; toluene; at 50 ℃; for 5h; Schlenk technique; Inert atmosphere;
DOI:10.1039/c3dt51377g

Reference yield: 72.0%

: 131063-11-1,16997-51-6,19559-06-9
Vanadium (III) chloride-(tris-tetrahydrofuran)

: 274687-50-2
2-(4-CF₃-C₆H₄-NCH)C₄H₃NH

: [2-(4-CF₃C₆H₄N=CH)C₄H₃N]VCl₂(THF)2

Guidance literature:: With n-C₄H₉Li; In tetrahydrofuran; hexane; (Ar); to stirred soln. of ligand in THF at -78°C, 2.5 M soln. of n-BuLi in hexane was added, allowed to warm to room temp., stirred for 2.5 h, soln. of VCl3(THF)3 in THF was added at -78°C, slowly warmed to r.t., stirred overnight; evapd. in vac., toluene was added, stirred for 10 min, filtered, filtrate was concd. in vac., crystd. by diffusion of n-hexane, elem. anal.;
DOI:10.1039/b909495d