3-O-benzyl-6-deoxy-1,2-O-isopropylidene-5-O-methylsulfonyl-α-D-allofuranose

Base Information

Chemical Name:3-O-benzyl-6-deoxy-1,2-O-isopropylidene-5-O-methylsulfonyl-α-D-allofuranose
CAS No.:117238-29-6
Molecular Formula:C₁₇H₂₄O₇S
Molecular Weight:372.439
Hs Code.:

Synonyms:3-O-benzyl-6-deoxy-1,2-O-isopropylidene-5-O-methylsulfonyl-α-D-allofuranose

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Chemical Property of 3-O-benzyl-6-deoxy-1,2-O-isopropylidene-5-O-methylsulfonyl-α-D-allofuranose

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Technology Process of 3-O-benzyl-6-deoxy-1,2-O-isopropylidene-5-O-methylsulfonyl-α-D-allofuranose

There total 10 articles about 3-O-benzyl-6-deoxy-1,2-O-isopropylidene-5-O-methylsulfonyl-α-D-allofuranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 124-63-0
methanesulfonyl chloride

: 70632-45-0
(R)-1-((3aR,5R,6R,6aR)-6-(benzyloxy)-2,2-dimethyltetrahydrofuro[2,3-d][1,3]dioxol-5-yl)ethanol

: 117238-29-6
3-O-benzyl-6-deoxy-1,2-O-isopropylidene-5-O-methylsulfonyl-α-D-allofuranose

Guidance literature:: With pyridine; for 1h; Ambient temperature;
DOI:10.1246/bcsj.67.236

Reference yield:

: 57099-04-4
3-O-benzyl-1,2-O-isopropylidene-α-D-allofuranose

: 117238-29-6
3-O-benzyl-6-deoxy-1,2-O-isopropylidene-5-O-methylsulfonyl-α-D-allofuranose

Guidance literature:: Multi-step reaction with 3 steps

1: 85 percent / pyridine

2: 94 percent / lithium triethylborohydride / tetrahydrofuran

3: 4-(diethylamino)pyridine / pyridine

With diethyl-pyridin-4-yl-amine; lithium triethylborohydride; In tetrahydrofuran; pyridine;
DOI:10.1039/c39880000483

Reference yield:

: 22331-21-1
1,2:5,6-di-O-isopropylidene-3-O-benzyl-α-D-allofuranose

: 117238-29-6
3-O-benzyl-6-deoxy-1,2-O-isopropylidene-5-O-methylsulfonyl-α-D-allofuranose

Guidance literature:: Multi-step reaction with 4 steps

1: acetic acid / H₂O

2: 85 percent / pyridine

3: 94 percent / lithium triethylborohydride / tetrahydrofuran

4: 4-(diethylamino)pyridine / pyridine

With diethyl-pyridin-4-yl-amine; lithium triethylborohydride; acetic acid; In tetrahydrofuran; pyridine; water;
DOI:10.1039/c39880000483