Mn⁽²⁺⁾*C₆H₃(OCH₃)OCHN(CH₂)3NCHC₆H₃(OCH₃)O^(2-) = (C₆H₃CH₃O(O)CHN(CH₂)3NCHC₆H₃CH₃O(O))Mn

Base Information

• Chemical Name: Mn⁽²⁺⁾*C₆H₃(OCH₃)OCHN(CH₂)3NCHC₆H₃(OCH₃)O^(2-) = (C₆H₃CH₃O(O)CHN(CH₂)3NCHC₆H₃CH₃O(O))Mn
• CAS No.: 143145-25-9
• Molecular Formula: C₁₉H₂₀N₂O₄*Mn
• Molecular Weight: 395.317

Synonyms:Mn⁽²⁺⁾*C₆H₃(OCH₃)OCHN(CH₂)3NCHC₆H₃(OCH₃)O^(2-) = (C₆H₃CH₃O(O)CHN(CH₂)3NCHC₆H₃CH₃O(O))Mn

Chemical Property of Mn⁽²⁺⁾*C₆H₃(OCH₃)OCHN(CH₂)3NCHC₆H₃(OCH₃)O^(2-) = (C₆H₃CH₃O(O)CHN(CH₂)3NCHC₆H₃CH₃O(O))Mn

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Technology Process of Mn⁽²⁺⁾*C₆H₃(OCH₃)OCHN(CH₂)3NCHC₆H₃(OCH₃)O^(2-) = (C₆H₃CH₃O(O)CHN(CH₂)3NCHC₆H₃CH₃O(O))Mn

There total 2 articles about Mn⁽²⁺⁾*C₆H₃(OCH₃)OCHN(CH₂)3NCHC₆H₃(OCH₃)O^(2-) = (C₆H₃CH₃O(O)CHN(CH₂)3NCHC₆H₃CH₃O(O))Mn which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

2-hydroxy-5-methoxybenzaldehyde (672-13-9) + manganese (II) acetate tetrahydrate (6156-78-1) + Trimethylenediamine (109-76-2,54018-94-9) → Mn(2+)*C6H3(OCH3)OCHN(CH2)3NCHC6H3(OCH3)O(2-) = (C6H3CH3O(O)CHN(CH2)3NCHC6H3CH3O(O))Mn (143145-25-9)

Guidance literature:

With potassium hydroxide; In methanol; water; refluxed for 30 min; soln. was cooled to room temp.; stirred for 1 h;; filtered, washed with water; dried at room temp. in vac. for 24 h; washed with hot acetonitrile; dried in vac.; elem. anal.;;

Reference yield:

2Mn(4+)*2(C6H3(OCH3)OCHN(CH2)3NCHC6H3(CH3O)O)(2-)*2O(2-) = {(C6H3(CH3O)(O)CHN(CH2)3NCHC6H3(CH3O)(O))Mn(O)}2 + N,N'-bis(salicylidene)ethylenediamine iron(II) (14167-12-5,578710-63-1) → Mn(2+)*C6H3(OCH3)OCHN(CH2)3NCHC6H3(OCH3)O(2-) = (C6H3CH3O(O)CHN(CH2)3NCHC6H3CH3O(O))Mn (143145-25-9) + {Fe(N,N'-ethylenebis(salicylideneimine)(2-))}2O

Guidance literature:

In N,N-dimethyl-formamide; under N2, color changed from red to deep red; not isolated, monitored by cyclovoltammetry;

Reference yield: 69.0%

Mn(2+)*C6H3(OCH3)OCHN(CH2)3NCHC6H3(OCH3)O(2-) = (C6H3CH3O(O)CHN(CH2)3NCHC6H3CH3O(O))Mn (143145-25-9) → 2Mn(4+)*2(C6H3(OCH3)OCHN(CH2)3NCHC6H3(CH3O)O)(2-)*2O(2-) = {(C6H3(CH3O)(O)CHN(CH2)3NCHC6H3(CH3O)(O))Mn(O)}2

Guidance literature:

With oxygen; In acetonitrile; reaction was complete after 15 min;; filtered in air; washed with acetonitrile; dried in vac.; recrystd. from a dichloromethane/petroleum ether mixture in air; elem. anal.;

upstream raw materials:

N,N'-bis(salicylidene)ethylenediamine iron(II)

2-hydroxy-5-methoxybenzaldehyde

manganese (II) acetate tetrahydrate

Trimethylenediamine

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