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6156-78-1

6156-78-1

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  • Good Price Top Quality Manganese (II) Acetate Tetrahydrate for Catalyst Hot Sales Manganese (II) Acetate Tetrahydrate Wholesale Price Manganese (II) Acetate Tetrahydrate in Stock

    Cas No: 6156-78-1

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6156-78-1 Usage

Chemical Properties

PALE PINK CRYSTALS

Uses

Manganese(II) acetate tetrahydrate may be used in the sol gel synthesis of doped TiO2 containing different amounts of Mn2+.

General Description

Manganese(II) acetate tetrahydrate is a hydrated salt of manganese. Kinetic studies suggest that its dehydration takes place in two-step reaction involving the loss of two water molecules. Its crystal structure has been investigated by X-ray studies. Its crystals exhibit monoclinic crystal system and space group P21/c.

Check Digit Verification of cas no

The CAS Registry Mumber 6156-78-1 includes 7 digits separated into 3 groups by hyphens. The first part of the number,starting from the left, has 4 digits, 6,1,5 and 6 respectively; the second part has 2 digits, 7 and 8 respectively.
Calculate Digit Verification of CAS Registry Number 6156-78:
(6*6)+(5*1)+(4*5)+(3*6)+(2*7)+(1*8)=101
101 % 10 = 1
So 6156-78-1 is a valid CAS Registry Number.
InChI:InChI=1/C2H4O2.Mn.4H2O/c1-2(3)4;;;;;/h1H3,(H,3,4);;4*1H2/q;+2;;;;/p-1

6156-78-1 Well-known Company Product Price

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  • Alfa Aesar

  • (10802)  Manganese(II) acetate tetrahydrate, Puratronic?, 99.999% (metals basis)   

  • 6156-78-1

  • 5g

  • 630.0CNY

  • Detail

  • Alfa Aesar

  • (10802)  Manganese(II) acetate tetrahydrate, Puratronic?, 99.999% (metals basis)   

  • 6156-78-1

  • 25g

  • 1948.0CNY

  • Detail

  • Alfa Aesar

  • (12351)  Manganese(II) acetate tetrahydrate, Mn 22% (typical)   

  • 6156-78-1

  • 100g

  • 209.0CNY

  • Detail

  • Alfa Aesar

  • (12351)  Manganese(II) acetate tetrahydrate, Mn 22% (typical)   

  • 6156-78-1

  • 500g

  • 350.0CNY

  • Detail

  • Alfa Aesar

  • (12351)  Manganese(II) acetate tetrahydrate, Mn 22% (typical)   

  • 6156-78-1

  • 2kg

  • 1045.0CNY

  • Detail

  • Sigma-Aldrich

  • (63537)  Manganese(II)acetatetetrahydrate  purum p.a., ≥99.0% (KT)

  • 6156-78-1

  • 63537-250G

  • 480.87CNY

  • Detail

  • Sigma-Aldrich

  • (63537)  Manganese(II)acetatetetrahydrate  purum p.a., ≥99.0% (KT)

  • 6156-78-1

  • 63537-1KG

  • 1,021.41CNY

  • Detail

  • Vetec

  • (V900089)  Manganese(II)acetatetetrahydrate  Vetec™ reagent grade, 98%

  • 6156-78-1

  • V900089-500G

  • 98.28CNY

  • Detail

  • Aldrich

  • (229776)  Manganese(II)acetatetetrahydrate  99.99% trace metals basis

  • 6156-78-1

  • 229776-50G

  • 1,872.00CNY

  • Detail

  • Aldrich

  • (221007)  Manganese(II)acetatetetrahydrate  ≥99%

  • 6156-78-1

  • 221007-25G

  • 424.71CNY

  • Detail

  • Aldrich

  • (221007)  Manganese(II)acetatetetrahydrate  ≥99%

  • 6156-78-1

  • 221007-500G

  • 492.57CNY

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  • Aldrich

  • (221007)  Manganese(II)acetatetetrahydrate  ≥99%

  • 6156-78-1

  • 221007-2KG

  • 1,654.38CNY

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6156-78-1SDS

SAFETY DATA SHEETS

According to Globally Harmonized System of Classification and Labelling of Chemicals (GHS) - Sixth revised edition

Version: 1.0

Creation Date: Aug 13, 2017

Revision Date: Aug 13, 2017

1.Identification

1.1 GHS Product identifier

Product name MANGANESE(II) ACETATE TETRAHYDRATE

1.2 Other means of identification

Product number -
Other names Acetic acid, manganese(2+) salt, tetrahydrate

1.3 Recommended use of the chemical and restrictions on use

Identified uses For industry use only.
Uses advised against no data available

1.4 Supplier's details

1.5 Emergency phone number

Emergency phone number -
Service hours Monday to Friday, 9am-5pm (Standard time zone: UTC/GMT +8 hours).

More Details:6156-78-1 SDS

6156-78-1Synthetic route

acetaldehyde
75-07-0

acetaldehyde

acetic acid
64-19-7

acetic acid

manganese (II) acetate tetrahydrate
6156-78-1

manganese (II) acetate tetrahydrate

Conditions
ConditionsYield
With manganese(IV) oxide; alkali cetate at 80℃;
With manganese(IV) oxide; alkaline earth acetate at 80℃;
C6H10(NCHC6H2C(CH3)3OHC15H10O(C(CH3)3)2)2(C6H4COOH)2

C6H10(NCHC6H2C(CH3)3OHC15H10O(C(CH3)3)2)2(C6H4COOH)2

manganese (II) acetate tetrahydrate
6156-78-1

manganese (II) acetate tetrahydrate

sodium chloride
7647-14-5

sodium chloride

MnCl(C6H10(NCHC6H2C(CH3)3OC15H10O(C(CH3)3)2)2(C6H4COOH)2)

MnCl(C6H10(NCHC6H2C(CH3)3OC15H10O(C(CH3)3)2)2(C6H4COOH)2)

Conditions
ConditionsYield
In ethanol xanthene-compound was added to Mn(CH3CO2)2*4H2O in abs. ethanol, the soln. was refluxed in air for 2 h, cooled, aq. satd. NaCl was added, the mixt. was stirred for 10 min; extd. with CH2Cl2, the organic layer was washed with water, dried over MgSO4, the solid was rotary evapd.; elem. anal.;100%
5-[2-chloro-6-[(18-crown-6)methyloxy]phenyl]-10,15,20-tri-(2,6-dichlorophenyl) porphyrin

5-[2-chloro-6-[(18-crown-6)methyloxy]phenyl]-10,15,20-tri-(2,6-dichlorophenyl) porphyrin

manganese (II) acetate tetrahydrate
6156-78-1

manganese (II) acetate tetrahydrate

Mn[5-[2-chloro-6-[(18-crown-6)methyloxy]phenyl]-10,15,20-tri-(2,6-dichlorophenyl) porphyrin](1+)
184765-61-5

Mn[5-[2-chloro-6-[(18-crown-6)methyloxy]phenyl]-10,15,20-tri-(2,6-dichlorophenyl) porphyrin](1+)

Conditions
ConditionsYield
In N,N-dimethyl-formamide stirring under reflux (4 h); solvent evapn. (vac.), dissolving in CH2Cl2, washing (water), chromy. (silica gel, CHCl3/EtOH), dissolving in CH2Cl2, stirring with NaCl soln., org. phase drying (MgSO4), solvent evapn.;100%
5-[2-chloro-6-[9-(18-crown-6)nonyloxy]phenyl]-10,15,20-tri-(2,6-dichlorophenyl) porphyrin

5-[2-chloro-6-[9-(18-crown-6)nonyloxy]phenyl]-10,15,20-tri-(2,6-dichlorophenyl) porphyrin

manganese (II) acetate tetrahydrate
6156-78-1

manganese (II) acetate tetrahydrate

Mn[5-[2-chloro-6-[9-(18-crown-6)nonyloxy]phenyl]-10,15,20-tri-(2,6-dichlorophenyl) porphyrin](1+)
184765-68-2

Mn[5-[2-chloro-6-[9-(18-crown-6)nonyloxy]phenyl]-10,15,20-tri-(2,6-dichlorophenyl) porphyrin](1+)

Conditions
ConditionsYield
In N,N-dimethyl-formamide stirring under reflux (4 h); solvent evapn. (vac.), dissolving in CH2Cl2, washing (water), chromy. (silica gel, CHCl3/EtOH), dissolving in CH2Cl2, stirring with NaCl soln., org. phase drying (MgSO4), solvent evapn.;100%
5-[2,6-dichloro-3-[9-(18-crown-6)nonyloxy]phenyl]-10,15,20-tri-(2,6-dichlorophenyl) porphyrin

5-[2,6-dichloro-3-[9-(18-crown-6)nonyloxy]phenyl]-10,15,20-tri-(2,6-dichlorophenyl) porphyrin

manganese (II) acetate tetrahydrate
6156-78-1

manganese (II) acetate tetrahydrate

Mn[5-[2,6-dichloro-3-[9-(18-crown-6)nonyloxy]phenyl]-10,15,20-tri-(2,6-dichlorophenyl) porphyrin](1+)
184765-75-1

Mn[5-[2,6-dichloro-3-[9-(18-crown-6)nonyloxy]phenyl]-10,15,20-tri-(2,6-dichlorophenyl) porphyrin](1+)

Conditions
ConditionsYield
In N,N-dimethyl-formamide stirring under reflux (4 h); solvent evapn. (vac.), dissolving in CH2Cl2, washing (water), chromy. (silica gel, CHCl3/EtOH), dissolving in CH2Cl2, stirring with NaCl soln., org. phase drying (MgSO4), solvent evapn.;100%
H2[C75H64Cl8N4O8]

H2[C75H64Cl8N4O8]

manganese (II) acetate tetrahydrate
6156-78-1

manganese (II) acetate tetrahydrate

Mn[C75H64Cl8N4O8](1+)
184765-80-8

Mn[C75H64Cl8N4O8](1+)

Conditions
ConditionsYield
In N,N-dimethyl-formamide stirring under reflux (4 h); solvent evapn. (vac.), dissolving in CH2Cl2, washing (water), chromy. (silica gel, CHCl3/EtOH), dissolving in CH2Cl2, stirring with NaCl soln., org. phase drying (MgSO4), solvent evapn.;100%
K4[Re6Se8(CN)6]·3.5H2O

K4[Re6Se8(CN)6]·3.5H2O

water
7732-18-5

water

manganese (II) acetate tetrahydrate
6156-78-1

manganese (II) acetate tetrahydrate

N,N-dimethyl-formamide
68-12-2, 33513-42-7

N,N-dimethyl-formamide

catena-(octakis(μ3-selenido)-hexakis(μ2-cyano)-hexarhenium(III)-aqua-bis(dimethylformamido)manganese(II))bis(dimethylformamide)

catena-(octakis(μ3-selenido)-hexakis(μ2-cyano)-hexarhenium(III)-aqua-bis(dimethylformamido)manganese(II))bis(dimethylformamide)

Conditions
ConditionsYield
In water; N,N-dimethyl-formamide soln. of K4(Re6Se8(CN)6)*3.5H2O (0.08 mmol) in H2O/DMF added to soln. ofMn(CH3COO)2*4H2O (0.18 mmol) in H2O/DMF under stirring, mixt. refluxed for 1 h, cooled; ppt. filtered off, washed twice with H2O/DMF and CH3CN, air-dried; elem.anal.;100%
4K(1+)*[Re6S8(CN)6](4-)=K4[Re6S8(CN)6]

4K(1+)*[Re6S8(CN)6](4-)=K4[Re6S8(CN)6]

water
7732-18-5

water

manganese (II) acetate tetrahydrate
6156-78-1

manganese (II) acetate tetrahydrate

N,N-dimethyl-formamide
68-12-2, 33513-42-7

N,N-dimethyl-formamide

catena-(octakis(μ3-sulfido)-hexakis(μ2-cyano)-hexarhenium(III)-aqua-bis(dimethylformamido)manganese(II))bis(dimethylformamide)

catena-(octakis(μ3-sulfido)-hexakis(μ2-cyano)-hexarhenium(III)-aqua-bis(dimethylformamido)manganese(II))bis(dimethylformamide)

Conditions
ConditionsYield
In water mixt. of H2O/DMF (75/1) added dropwise to aq. soln. of K4(Re6S8(CN)6) (0.029 mmol) and Mn(CH3COO)2*4H2O (0.068 mmol) under stirring; soln. concd., stored in air for a week, crystals filtered off, washed twice (CH3CN), air-dried; elem. anal.;100%
4Cs(1+)*Re6Te8(CN)6(4-) = Cs4[Re6Te8(CN)6]

4Cs(1+)*Re6Te8(CN)6(4-) = Cs4[Re6Te8(CN)6]

water
7732-18-5

water

manganese (II) acetate tetrahydrate
6156-78-1

manganese (II) acetate tetrahydrate

N,N-dimethyl-formamide
68-12-2, 33513-42-7

N,N-dimethyl-formamide

catena-(octakis(μ3-tellurido)-hexakis(μ2-cyano)-hexarhenium(III)-aqua-bis(dimethylformamido)manganese(II))bis(dimethylformamide)

catena-(octakis(μ3-tellurido)-hexakis(μ2-cyano)-hexarhenium(III)-aqua-bis(dimethylformamido)manganese(II))bis(dimethylformamide)

Conditions
ConditionsYield
In water; N,N-dimethyl-formamide soln. of Cs4(Re6Te8(CN)6) (0.08 mmol) in H2O/DMF slowly added to soln. of Mn(CH3COO)2*4H2O (0.18 mmol) in H2O/DMF under stirring, mixt. refluxedfor 1 h, cooled; ppt. filtered off, washed with H2O/DMF and CH3CN, air-dried; elem. anal.;100%
K4[Re6Se8(CN)6]·3.5H2O

K4[Re6Se8(CN)6]·3.5H2O

manganese (II) acetate tetrahydrate
6156-78-1

manganese (II) acetate tetrahydrate

N,N-dimethyl-formamide
68-12-2, 33513-42-7

N,N-dimethyl-formamide

catena-(octakis(μ3-selenido)-hexakis(μ2-cyano)-hexarhenium(III)-tris(dimethylformamido)manganese(II))

catena-(octakis(μ3-selenido)-hexakis(μ2-cyano)-hexarhenium(III)-tris(dimethylformamido)manganese(II))

Conditions
ConditionsYield
In water; N,N-dimethyl-formamide soln. of K4(Re6Se8(CN)6)*3.5H2O in H2O/DMF added to soln. of Mn(CH3COO)2*4H2O in H2O/DMF with vigorous stirring, mixt. stirred for 2 h; ppt. filtered off, washed twice with H2O/DMF (1/1) and CH3CN, air-dried;elem. anal.;100%
bis(tetrabutylammonium) {(o-phenylenebis(oxamato))copper(II)}

bis(tetrabutylammonium) {(o-phenylenebis(oxamato))copper(II)}

manganese (II) acetate tetrahydrate
6156-78-1

manganese (II) acetate tetrahydrate

bis(tetrabutylammonium)oxalate
33081-83-3

bis(tetrabutylammonium)oxalate

(tetrabutylammonium)2[Mn2{Cu(1,2-phenylenebis(oxamate))}2(oxalate)]

(tetrabutylammonium)2[Mn2{Cu(1,2-phenylenebis(oxamate))}2(oxalate)]

Conditions
ConditionsYield
In water; dimethyl sulfoxide at 20℃; for 730.5h;100%
manganese(II) acetate dihydrate

manganese(II) acetate dihydrate

manganese (II) acetate tetrahydrate
6156-78-1

manganese (II) acetate tetrahydrate

zinc manganite

zinc manganite

Conditions
ConditionsYield
In water at 500℃; Green chemistry;100%
manganese (II) acetate tetrahydrate
6156-78-1

manganese (II) acetate tetrahydrate

1,10-phenanthroline hydrate
5144-89-8

1,10-phenanthroline hydrate

{Mn3(O2CCH3)6(1,10-phenanthroline)2}

{Mn3(O2CCH3)6(1,10-phenanthroline)2}

Conditions
ConditionsYield
In N,N-dimethyl-formamide stirred for 10 min; filtered, washed with DMF, acetone and diethyl ether, dried in vac.; elem. anal.;99%
sodium azide

sodium azide

manganese (II) acetate tetrahydrate
6156-78-1

manganese (II) acetate tetrahydrate

meso-tetrakis(pentafluorophenyl)-β-octachloroporphyrinatomanganese(III) azide
170463-43-1

meso-tetrakis(pentafluorophenyl)-β-octachloroporphyrinatomanganese(III) azide

Conditions
ConditionsYield
In methanol; acetone (N2); soln. stiring (room temp., 12 h); filtration, solvent removal (rotary evapn.), solid redissolving (CH2Cl2), washing (water), org. layer drying (Na2SO4), solvent removal (rotary evapn.), drying (vac., overnight, room temp.);99%
2N((CH2)3CH3)4(1+)*Mo2O5(O2C6H2(NCHC6H3(OC2H5)OH)2)2(2-)=[N((CH2)3CH3)4]2[Mo2O5(O2C6H2(NCHC6H3(OC2H5)OH)2)2]

2N((CH2)3CH3)4(1+)*Mo2O5(O2C6H2(NCHC6H3(OC2H5)OH)2)2(2-)=[N((CH2)3CH3)4]2[Mo2O5(O2C6H2(NCHC6H3(OC2H5)OH)2)2]

manganese (II) acetate tetrahydrate
6156-78-1

manganese (II) acetate tetrahydrate

2N((CH2)3CH3)4(1+)*Mo2O5(O2C6H2(NCHC6H3(OC2H5)O)2Mn)2(2-)=[N((CH2)3CH3)4]2[Mo2O5(O2C6H2(NCHC6H3(OC2H5)O)2Mn)2]

2N((CH2)3CH3)4(1+)*Mo2O5(O2C6H2(NCHC6H3(OC2H5)O)2Mn)2(2-)=[N((CH2)3CH3)4]2[Mo2O5(O2C6H2(NCHC6H3(OC2H5)O)2Mn)2]

Conditions
ConditionsYield
In methanol; acetone byproducts: H2O; inert atmosphere; dropwise addn. of metal acetate (in MeOH) to 0.5 equiv. Mn-complex (in Me2CO), stirring for 1 h; solvent removal (vac.), dissoln. in THF/CH2Cl2=10:1, pptn. on Et2O addn., standing overnight;99%
manganese (II) acetate tetrahydrate
6156-78-1

manganese (II) acetate tetrahydrate

bis(acetato)manganese(II)

bis(acetato)manganese(II)

Conditions
ConditionsYield
In acetonitrile evacuated sealed ampoule (150°C, 6 weeks); elem. anal.;99%
In acetonitrile High Pressure; Mn(CH3COO)2*4H2O dehydrated in acetonitrile at 150°C for 6 weeks;99%
5-(2-chloro-6-{(ethoxycarbonyl)methoxy}phenyl)-10,15,20-tris(2,6-dichlorophenyl)porphyrin

5-(2-chloro-6-{(ethoxycarbonyl)methoxy}phenyl)-10,15,20-tris(2,6-dichlorophenyl)porphyrin

manganese (II) acetate tetrahydrate
6156-78-1

manganese (II) acetate tetrahydrate

5-{2-(OOC-methoxy)-6-chlorophenyl}-10,15,20-tris(2,6-dichlorophenyl)porphyrin Mn(III)
749180-71-0, 151421-96-4

5-{2-(OOC-methoxy)-6-chlorophenyl}-10,15,20-tris(2,6-dichlorophenyl)porphyrin Mn(III)

Conditions
ConditionsYield
In N,N-dimethyl-formamide a soln. of porphyrin-compd. in DMF is stirred at reflux with Mn(OAc)2*4H2O for 6 h; evapn. under reduced pressure, the residue is dissolved in in CH2Cl2 and washed with water, evapn., the residue is dissolved in EtOH and NaOH and refluxed for 2 h, evapn., addn. of H2O and HCl, extn. with CH2Cl2, column chromy., dried over MgSO4;99%
(1S,2S)-N-(5-benzoylthio-3-tert-butylsalicylidene)-N'-(3,5-di-tert-butylsalicylidene)-1,2-diphenylethylenediamine

(1S,2S)-N-(5-benzoylthio-3-tert-butylsalicylidene)-N'-(3,5-di-tert-butylsalicylidene)-1,2-diphenylethylenediamine

manganese (II) acetate tetrahydrate
6156-78-1

manganese (II) acetate tetrahydrate

sodium chloride
7647-14-5

sodium chloride

MnCl(OC6H2(C(CH3)3)(SC(O)C6H5)CHNCH(C6H5)CH(C6H5)NCHC6H2(C(CH3)3)2O)

MnCl(OC6H2(C(CH3)3)(SC(O)C6H5)CHNCH(C6H5)CH(C6H5)NCHC6H2(C(CH3)3)2O)

Conditions
ConditionsYield
With air In methanol Mn compd. added to soln. of ligand (molar ratio 2:1) in MeOH; stirred for 30 min at 50°C; brine added; stirred for 30 min at 50°C; solvent evapd. in vac.; dissolved in CH2Cl2; washed with brine and H2O; org. phase dried over Na2SO4; evapd. in vac.;99%
(1S,2S)-N-(5-(2-[4-(acetylthio)phenyl]ethynyl)-3-tert-butylsalicylidene)-N'-(3,5-di-tert-butylsalicylidene)-1,2-diphenylethylenediamine

(1S,2S)-N-(5-(2-[4-(acetylthio)phenyl]ethynyl)-3-tert-butylsalicylidene)-N'-(3,5-di-tert-butylsalicylidene)-1,2-diphenylethylenediamine

manganese (II) acetate tetrahydrate
6156-78-1

manganese (II) acetate tetrahydrate

sodium chloride
7647-14-5

sodium chloride

MnCl(OC6H2(C(CH3)3)(C2C6H4SC(O)CH3)CHNCH(C6H5)CH(C6H5)NCHC6H2(C(CH3)3)2O)

MnCl(OC6H2(C(CH3)3)(C2C6H4SC(O)CH3)CHNCH(C6H5)CH(C6H5)NCHC6H2(C(CH3)3)2O)

Conditions
ConditionsYield
With air In methanol Mn compd. added to soln. of ligand (molar ratio 2:1) in MeOH; stirred for 30 min at 50°C; brine added; stirred for 30 min at 50°C; solvent evapd. in vac.; dissolved in CH2Cl2; washed with brine and H2O; org. phase dried over Na2SO4; evapd. in vac.;99%
(1S,2S)-N-(5-[2-(4-(2-[4-(acetylthio)phenyl]ethynyl)phenyl)ethynyl]-3-tert-butylsalicylidene)-N'-(3,5-di-tert-butylsalicylidene)-1,2-diphenylethylenediamine

(1S,2S)-N-(5-[2-(4-(2-[4-(acetylthio)phenyl]ethynyl)phenyl)ethynyl]-3-tert-butylsalicylidene)-N'-(3,5-di-tert-butylsalicylidene)-1,2-diphenylethylenediamine

manganese (II) acetate tetrahydrate
6156-78-1

manganese (II) acetate tetrahydrate

sodium chloride
7647-14-5

sodium chloride

MnCl(OC6H2(C(CH3)3)((C2C6H4)2SC(O)CH3)CHNCH(C6H5)CH(C6H5)NCHC6H2(C(CH3)3)2O)

MnCl(OC6H2(C(CH3)3)((C2C6H4)2SC(O)CH3)CHNCH(C6H5)CH(C6H5)NCHC6H2(C(CH3)3)2O)

Conditions
ConditionsYield
With air In methanol Mn compd. added to soln. of ligand (molar ratio 2:1) in MeOH; stirred for 30 min at 50°C; brine added; stirred for 30 min at 50°C; solvent evapd. in vac.; dissolved in CH2Cl2; washed with brine and H2O; org. phase dried over Na2SO4; evapd. in vac.;99%
pyridine
110-86-1

pyridine

manganese (II) acetate tetrahydrate
6156-78-1

manganese (II) acetate tetrahydrate

1,3-bis-(3-oxo-3-phenyl-propionyl)-2-hydroxy-5-methylbenzene
377736-65-7

1,3-bis-(3-oxo-3-phenyl-propionyl)-2-hydroxy-5-methylbenzene

Mn2((C6H5COCHCO)2CH3C6H2OH)2(C5H5N)4

Mn2((C6H5COCHCO)2CH3C6H2OH)2(C5H5N)4

Conditions
ConditionsYield
In pyridine to a stirred soln. of Mn-salt in pyridine was added a soln. of tetraketone in pyridine, stirred for a few min (inert atm.); diethyl ether was added, the flask was stopped and left undisturbed for 2 days, crystals were filtered, dried in vac.; elem. anal.;99%
(C8F17)2C6H2(OH)CHNC6H10NCHC6H2(OH)(C8F17)2

(C8F17)2C6H2(OH)CHNC6H10NCHC6H2(OH)(C8F17)2

manganese (II) acetate tetrahydrate
6156-78-1

manganese (II) acetate tetrahydrate

Mn(C8F17)2C6H2(O)CHNC6H10NCHC6H2(O)(C8F17)2

Mn(C8F17)2C6H2(O)CHNC6H10NCHC6H2(O)(C8F17)2

Conditions
ConditionsYield
In ethanol refluxing;99%
(C8F17)2C6H2(OH)CHNCH(C6H5)CH(C6H5)NCHC6H2(OH)(C8F17)2

(C8F17)2C6H2(OH)CHNCH(C6H5)CH(C6H5)NCHC6H2(OH)(C8F17)2

manganese (II) acetate tetrahydrate
6156-78-1

manganese (II) acetate tetrahydrate

Mn(C8F17)2C6H2(O)CHNCH(C6H5)CH(C6H5)NCHC6H2(O)(C8F17)2

Mn(C8F17)2C6H2(O)CHNCH(C6H5)CH(C6H5)NCHC6H2(O)(C8F17)2

Conditions
ConditionsYield
In ethanol refluxing;99%
4Cs(1+)*Re6Te8(CN)6(4-)*3H2O=Cs4Re6Te8(CN)6*3H2O

4Cs(1+)*Re6Te8(CN)6(4-)*3H2O=Cs4Re6Te8(CN)6*3H2O

manganese (II) acetate tetrahydrate
6156-78-1

manganese (II) acetate tetrahydrate

ethylenediamine
107-15-3

ethylenediamine

[Mn(H2O)bis(ethylenediamine)][Mn bis(ethylenediamine)]2 Re6Te8(CN)6 (H2O)3

[Mn(H2O)bis(ethylenediamine)][Mn bis(ethylenediamine)]2 Re6Te8(CN)6 (H2O)3

Conditions
ConditionsYield
In water; glycerol Re complex in H2O layered on top of Mn salt and ethylenediamine in glycerol, crystd. for 2 weeks; filtered, dried, elem. anal.;99%
C6H10(NCHC6H2C(CH3)3OHC15H10O(C(CH3)3)2)2(COOH)2

C6H10(NCHC6H2C(CH3)3OHC15H10O(C(CH3)3)2)2(COOH)2

manganese (II) acetate tetrahydrate
6156-78-1

manganese (II) acetate tetrahydrate

sodium chloride
7647-14-5

sodium chloride

MnCl(C6H10(NCHC6H2C(CH3)3OC15H10O(C(CH3)3)2)2(COOH)2)

MnCl(C6H10(NCHC6H2C(CH3)3OC15H10O(C(CH3)3)2)2(COOH)2)

Conditions
ConditionsYield
In ethanol xanthene-compound was added to Mn(CH3CO2)2*4H2O in abs. ethanol, the soln. was refluxed in air for 2 h, cooled, aq. satd. NaCl was added, the mixt. was stirred for 10 min; extd. with CH2Cl2, the organic layer was washed with water, dried over MgSO4, the solid was rotary evapd.; elem. anal.;99%
N,N'-ethylenebis(2-hydroxybenzylimine)-5,5'-dicarboxylic acid

N,N'-ethylenebis(2-hydroxybenzylimine)-5,5'-dicarboxylic acid

water
7732-18-5

water

manganese (II) acetate tetrahydrate
6156-78-1

manganese (II) acetate tetrahydrate

diaqua(N,N'-ethylenebis(2-oxybenzylimine)-5,5'-dicarboxylate)manganese(III) pentahydrate

diaqua(N,N'-ethylenebis(2-oxybenzylimine)-5,5'-dicarboxylate)manganese(III) pentahydrate

Conditions
ConditionsYield
In ethanol High Pressure; heated at 80°C for 3 h;99%
titanium(IV) isopropylate
546-68-9

titanium(IV) isopropylate

dichloromethane
75-09-2

dichloromethane

C92H72N2O6

C92H72N2O6

manganese (II) acetate tetrahydrate
6156-78-1

manganese (II) acetate tetrahydrate

lithium chloride

lithium chloride

C92H66N2O6(6-)*Ti(4+)*Mn(3+)*Cl(1-)*3CH2Cl2

C92H66N2O6(6-)*Ti(4+)*Mn(3+)*Cl(1-)*3CH2Cl2

Conditions
ConditionsYield
Stage #1: C92H72N2O6; manganese (II) acetate tetrahydrate With air In ethanol for 0.5h; Reflux;
Stage #2: lithium chloride In ethanol for 0.5h; Reflux;
Stage #3: titanium(IV) isopropylate; dichloromethane Further stages;		99%
manganese (II) acetate tetrahydrate
6156-78-1

manganese (II) acetate tetrahydrate

(R,R)-N,N'-bis(3,5-di-tert-butylsalicylidene)-1,2-cyclohexanediamine
135616-40-9

(R,R)-N,N'-bis(3,5-di-tert-butylsalicylidene)-1,2-cyclohexanediamine

sodium chloride
7647-14-5

sodium chloride

(-)-chloro((1R,2R)-4,4',6,6'-tetra-tert-butyl-2,2'-[cyclohexane-1,2-diylbis(nitrilomethylidyne)]diphenolato)manganese(III)
138124-32-0

(-)-chloro((1R,2R)-4,4',6,6'-tetra-tert-butyl-2,2'-[cyclohexane-1,2-diylbis(nitrilomethylidyne)]diphenolato)manganese(III)

Conditions
ConditionsYield
Stage #1: manganese (II) acetate tetrahydrate; (R,R)-N,N'-bis(3,5-di-tert-butylsalicylidene)-1,2-cyclohexanediamine In ethanol; toluene for 2.75h; Reflux;
Stage #2: With air In ethanol; toluene for 1h; Reflux;
Stage #3: sodium chloride In ethanol; water; toluene		99%
titanium(IV) isopropylate
546-68-9

titanium(IV) isopropylate

C92H74N2O5

C92H74N2O5

manganese (II) acetate tetrahydrate
6156-78-1

manganese (II) acetate tetrahydrate

lithium chloride

lithium chloride

C92H74N2O6*Ti*Mn*Cl

C92H74N2O6*Ti*Mn*Cl

Conditions
ConditionsYield
Stage #1: C92H74N2O5; manganese (II) acetate tetrahydrate In ethanol for 1h; Schlenk technique; Reflux;
Stage #2: lithium chloride In ethanol for 1h; Schlenk technique; Reflux;
Stage #3: titanium(IV) isopropylate In ethanol at 20℃; for 12h; Schlenk technique;		99%
5-(2-chloro-6-{7-(ethoxycarbonyl)heptyloxy}phenyl)-10,15,20-tris(2,6-dichlorophenyl)porphyrin

5-(2-chloro-6-{7-(ethoxycarbonyl)heptyloxy}phenyl)-10,15,20-tris(2,6-dichlorophenyl)porphyrin

manganese (II) acetate tetrahydrate
6156-78-1

manganese (II) acetate tetrahydrate

5-{2-(7-OOC-heptyloxy)-6-chlorophenyl}-10,15,20-tris(2,6-dichlorophenyl)porphyrin Mn(III)
151422-07-0

5-{2-(7-OOC-heptyloxy)-6-chlorophenyl}-10,15,20-tris(2,6-dichlorophenyl)porphyrin Mn(III)

Conditions
ConditionsYield
In N,N-dimethyl-formamide a soln. of porphyrin-compd. in DMF is stirred at reflux with Mn(OAc)2*4H2O for 6 h; evapn. under reduced pressure, the residue is dissolved in in CH2Cl2 and washed with water, evapn., the residue is dissolved in EtOH and NaOH and refluxed for 2 h, evapn., addn. of H2O and HCl, extn. with CH2Cl2, column chromy., dried over MgSO4;98%
C6H10(NCHC6H2C(CH3)3OHC15H10O(C(CH3)3)2)2(COOCH3)2

C6H10(NCHC6H2C(CH3)3OHC15H10O(C(CH3)3)2)2(COOCH3)2

manganese (II) acetate tetrahydrate
6156-78-1

manganese (II) acetate tetrahydrate

sodium chloride
7647-14-5

sodium chloride

MnCl(C6H10(NCHC6H2C(CH3)3OC15H10O(C(CH3)3)2)2(COOCH3)2)

MnCl(C6H10(NCHC6H2C(CH3)3OC15H10O(C(CH3)3)2)2(COOCH3)2)

Conditions
ConditionsYield
In ethanol xanthene-compound was added to Mn(CH3CO2)2*4H2O in abs. ethanol, the soln. was refluxed in air for 2 h, cooled, aq. satd. NaCl was added, the mixt. was stirred for 10 min; extd. with CH2Cl2, the organic layer was washed with water, dried over MgSO4, the solid was rotary evapd.; elem. anal.;98%
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