C₂₂H₃₄N₂O₆

Base Information

Chemical Name:C₂₂H₃₄N₂O₆
CAS No.:1357008-29-7
Molecular Formula:C₂₂H₃₄N₂O₆
Molecular Weight:422.522
Hs Code.:

C<sub>22</sub>H<sub>34</sub>N<sub>2</sub>O<sub>6</sub>

Synonyms:C₂₂H₃₄N₂O₆

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Chemical Property of C₂₂H₃₄N₂O₆

Chemical Property:

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Technology Process of C₂₂H₃₄N₂O₆

There total 1 articles about C₂₂H₃₄N₂O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 46460-82-6,55895-87-9,84907-81-3
O-benzyl-L-serine methyl ester

: 45170-31-8
Boc-N-Me-Val-OH

: 1357008-29-7
C₂₂H₃₄N₂O₆

Guidance literature:: With O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃; for 1h; Inert atmosphere;
DOI:10.1016/j.tet.2011.11.089

Reference yield:

: 1357008-29-7
C₂₂H₃₄N₂O₆

: 1357007-74-9
C₄₀H₄₇N₅O₆

Guidance literature:: Multi-step reaction with 9 steps

1.1: palladium on activated charcoal; hydrogen / ethanol / 24 h

2.1: diethylamino-sulfur trifluoride / dichloromethane / 1 h / -78 °C / Inert atmosphere

2.2: -78 - 20 °C

3.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / dichloromethane / 0.33 h / -47 °C / Inert atmosphere

3.2: -47 - 20 °C

4.1: methoxybenzene; trifluoroacetic acid / dichloromethane / 0.5 h

5.1: O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine; HATU / dichloromethane / 1.5 h / 20 °C / Inert atmosphere

6.1: dihydrogen peroxide; lithium hydroxide / methanol / 3 h / 20 °C

6.2: pH 1

7.1: methoxybenzene; trifluoroacetic acid / dichloromethane / 0.67 h

8.1: O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine; HATU; 3-[(diethoxyphosphinyl)oxy]-1,2,3-benzotriazin-4(3H)-one / dichloromethane; acetonitrile / 12 h

9.1: sodium hydride / tetrahydrofuran; N,N-dimethyl-formamide / 12 h / 20 °C / Inert atmosphere

With diethylamino-sulfur trifluoride; palladium on activated charcoal; hydrogen; dihydrogen peroxide; sodium hydride; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; methoxybenzene; 1,8-diazabicyclo[5.4.0]undec-7-ene; N-ethyl-N,N-diisopropylamine; HATU; trifluoroacetic acid; 3-[(diethoxyphosphinyl)oxy]-1,2,3-benzotriazin-4(3H)-one; lithium hydroxide; In tetrahydrofuran; methanol; ethanol; dichloromethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/j.tet.2011.11.089

Reference yield:

: 1357008-29-7
C₂₂H₃₄N₂O₆

: 1357008-32-2
C₃₉H₅₃N₅O₉

Guidance literature:: Multi-step reaction with 5 steps

1.1: palladium on activated charcoal; hydrogen / ethanol / 24 h

2.1: diethylamino-sulfur trifluoride / dichloromethane / 1 h / -78 °C / Inert atmosphere

2.2: -78 - 20 °C

3.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / dichloromethane / 0.33 h / -47 °C / Inert atmosphere

3.2: -47 - 20 °C

4.1: methoxybenzene; trifluoroacetic acid / dichloromethane / 0.5 h

5.1: O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine; HATU / dichloromethane / 1.5 h / 20 °C / Inert atmosphere

With diethylamino-sulfur trifluoride; palladium on activated charcoal; hydrogen; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; methoxybenzene; 1,8-diazabicyclo[5.4.0]undec-7-ene; N-ethyl-N,N-diisopropylamine; HATU; trifluoroacetic acid; In ethanol; dichloromethane;
DOI:10.1016/j.tet.2011.11.089