1-carbophenoxy-N-(methylsulfonyl)-1H-naphth<2,3-d>imidazole-6,7-dicarboximide

Base Information

Chemical Name:1-carbophenoxy-N-(methylsulfonyl)-1H-naphth<2,3-d>imidazole-6,7-dicarboximide
CAS No.:90108-78-4
Molecular Formula:C₂₁H₁₃N₃O₇S
Molecular Weight:451.416
Hs Code.:

Synonyms:1-carbophenoxy-N-(methylsulfonyl)-1H-naphth<2,3-d>imidazole-6,7-dicarboximide

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Chemical Property of 1-carbophenoxy-N-(methylsulfonyl)-1H-naphth<2,3-d>imidazole-6,7-dicarboximide

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Technology Process of 1-carbophenoxy-N-(methylsulfonyl)-1H-naphth<2,3-d>imidazole-6,7-dicarboximide

There total 5 articles about 1-carbophenoxy-N-(methylsulfonyl)-1H-naphth<2,3-d>imidazole-6,7-dicarboximide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 90108-77-3
1-carbophenoxy-N-hydroxy-1H-naphth<2,3-d>imidazole-6,7-dicarboximide

: 124-63-0
methanesulfonyl chloride

: 90108-78-4
1-carbophenoxy-N-(methylsulfonyl)-1H-naphth<2,3-d>imidazole-6,7-dicarboximide

Guidance literature:: With pyridine; In N,N-dimethyl acetamide; at 100 ℃; for 1h;
DOI:10.1021/jo00186a016

Reference yield:

: 582-60-5
5,6-dimethyl-1H-benzo[d]imida-zole

: 90108-78-4
1-carbophenoxy-N-(methylsulfonyl)-1H-naphth<2,3-d>imidazole-6,7-dicarboximide

Guidance literature:: Multi-step reaction with 4 steps

1: 71 percent / triethylamine / CH₂Cl₂ / 1 h / Ambient temperature

2: N-bromosuccinimide, benzoylperoxide / CCl₄ / Heating; Irradiation

3: 1.2 g / sodium iodide / dimethylformamide / 1.25 h / 80 °C / 100 Torr

4: 87 percent / pyridine / N,N-dimethyl-acetamide / 1 h / 100 °C

With pyridine; N-Bromosuccinimide; Perbenzoic acid; triethylamine; sodium iodide; In tetrachloromethane; dichloromethane; N,N-dimethyl acetamide; N,N-dimethyl-formamide;
DOI:10.1021/jo00186a016

Reference yield:

: 90108-69-3
1-carbophenoxy-5,6-dimethyl-1H-benzimidazole

: 90108-78-4
1-carbophenoxy-N-(methylsulfonyl)-1H-naphth<2,3-d>imidazole-6,7-dicarboximide

Guidance literature:: Multi-step reaction with 3 steps

1: N-bromosuccinimide, benzoylperoxide / CCl₄ / Heating; Irradiation

2: 1.2 g / sodium iodide / dimethylformamide / 1.25 h / 80 °C / 100 Torr

3: 87 percent / pyridine / N,N-dimethyl-acetamide / 1 h / 100 °C

With pyridine; N-Bromosuccinimide; Perbenzoic acid; sodium iodide; In tetrachloromethane; N,N-dimethyl acetamide; N,N-dimethyl-formamide;
DOI:10.1021/jo00186a016