Decanethioamide, N,N-dimethyl-

Base Information

• Chemical Name: Decanethioamide, N,N-dimethyl-
• CAS No.: 125188-67-2
• Molecular Formula: C12H25 N S
• Molecular Weight: 215.403
• Mol file: 125188-67-2.mol

Synonyms:Decanethioamide, N,N-dimethyl-

Chemical Property of Decanethioamide, N,N-dimethyl-

Chemical Property:

• Boiling Point: 84 °C (1 mmHg)
• PSA: 35.33000
• LogP: 4.01610

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Decanethioamide, N,N-dimethyl-

There total 2 articles about Decanethioamide, N,N-dimethyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

4-decyne (2384-86-3) + N,N-dimethyl-formamide (68-12-2,33513-42-7) → N,N-dimethyl decanethioamide (125188-67-2)

Guidance literature:

With sulfur; triphenylphosphine; cobalt acetylacetonate; at 130 ℃; for 6h;

DOI:10.1007/BF00957154

Reference yield: 57.0%

5-decyne (1942-46-7) + N,N-dimethyl-formamide (68-12-2,33513-42-7) → N,N-dimethyl decanethioamide (125188-67-2)

Guidance literature:

With sulfur; triphenylphosphine; cobalt acetylacetonate; at 130 ℃; for 6h; 130 deg C, 6h;

DOI:10.1007/BF00957154

Reference yield: 76.0%

N,N-dimethyl decanethioamide (125188-67-2) + carbonic acid 1,1-dimethylethyl 1,3-phenyl-2(E)-propenyl ester (121440-73-1) → C27H37NS

Guidance literature:

N,N-dimethyl decanethioamide; With (R)-(+)-2,2'-bis[bis(3,5-dimethylphenyl)phosphino]-1,1'-binaphthyl; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; sodium hexamethyldisilazane; In tetrahydrofuran; at 20 ℃; for 0.5h; Inert atmosphere; Molecular sieve;

carbonic acid 1,1-dimethylethyl 1,3-phenyl-2(E)-propenyl ester; In tetrahydrofuran; at 20 ℃; stereoselective reaction; Inert atmosphere; Molecular sieve;

DOI:10.1016/j.tetlet.2014.12.031

upstream raw materials:

5-decyne

N,N-dimethyl-formamide

4-decyne

Downstream raw materials:

C₁₈H₂₉NS

C₁₉H₃₁NS

C₂₂H₃₇NS

C₁₉H₃₁NS