4'-Bromononanophenone, 98%

Base Information

• Chemical Name: 4'-Bromononanophenone, 98%
• CAS No.: 126334-26-7
• Molecular Formula: C15H21 Br O
• Molecular Weight: 297.23
• Mol file: 126334-26-7.mol

Synonyms:1-Bromo-4-nonanoylbenzene

Chemical Property of 4'-Bromononanophenone, 98%

Chemical Property:

• Melting Point: 67-69°C
• Refractive Index: 1.516
• Boiling Point: 138-140°C/0.1mm
• Flash Point: 12.3°C
• PSA: 17.07000
• Density: 1.176g/cm³
• LogP: 5.38240

Purity/Quality:

98%,99%, ^*data from raw suppliers

1-(4-Bromo-phenyl)-nonan-1-one ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4'-Bromononanophenone, 98%

There total 5 articles about 4'-Bromononanophenone, 98% which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

bromobenzene (108-86-1,52753-63-6) + Nonanoyl chloride (764-85-2) → 1-(4-bromophenyl)nonan-1-one (126334-26-7)

Guidance literature:

With aluminium trichloride; 0 deg C, 1 h then 80 deg C, 2 h;

Reference yield: 96.0%

1-(4-bromophenyl)-1-hydroxynonane (76287-56-4) → 1-(4-bromophenyl)nonan-1-one (126334-26-7)

Guidance literature:

With pyridinium chlorochromate; In dichloromethane; at 20 ℃; for 2h;

Reference yield: 50.0%

1-Iodooctane (629-27-6) + carbon monoxide (201230-82-2) + 2-(4-bromophenyl)-5,5-dimethyl-1,3,2-dioxaborinane (183677-71-6) → 1-(4-bromophenyl)nonan-1-one (126334-26-7)

Guidance literature:

With chloro[1,3-bis(2,6-di-i-propylphenyl)imidazol-2-ylidene]copper(I); sodium pentacarbonyl manganate; potassium methanolate; In tetrahydrofuran; at 60 ℃; for 15h; under 2280.15 Torr;

DOI:10.1039/c7sc01170a

upstream raw materials:

bromobenzene

Nonanoyl chloride

1-(4-bromophenyl)-1-hydroxynonane

oct-1-ene

Downstream raw materials:

α-<4-Brom-phenyl>nonylamin

4-bromo-1-(1-nonyl)benzene