2,3-Diamino-4-methoxypyridine

Base Information

Chemical Name:2,3-Diamino-4-methoxypyridine
CAS No.:127356-16-5
Molecular Formula:C6H9 N3 O
Molecular Weight:139.157
Hs Code.:
DSSTox Substance ID:DTXSID40436763
Wikidata:Q82252065
Mol file:127356-16-5.mol

Synonyms:2,3-Diamino-4-methoxypyridine;127356-16-5;4-methoxypyridine-2,3-diamine;2,3-Pyridinediamine,4-methoxy-(9CI);4-methoxy-pyridine-2,3-diamine;2,3-Pyridinediamine, 4-methoxy-;4-methoxy-2,3-pyridinediamine;SCHEMBL2954177;DTXSID40436763;UYMYMHQOWIHQKU-UHFFFAOYSA-N;CFA35616;AKOS006307840;(2-amino-4-methoxy-pyridin-3-yl)-amine;AM20050746;CS-0443848;FT-0757397

Suppliers and Price of 2,3-Diamino-4-methoxypyridine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Chemcia Scientific
4-Methoxy-pyridine-2,3-diamine 95%
0.5 G
$ 320.00

American Custom Chemicals Corporation
2,3-DIAMINO-4-METHOXYPYRIDINE 95.00%
5MG
$ 504.66

Alichem
2,3-Diamino-4-methoxypyridine
1g
$ 3039.75

Alichem
2,3-Diamino-4-methoxypyridine
500mg
$ 1786.10

Alichem
2,3-Diamino-4-methoxypyridine
250mg
$ 970.20

Total 4 raw suppliers

Chemical Property of 2,3-Diamino-4-methoxypyridine

Chemical Property:

Boiling Point:335.1±37.0 °C(Predicted)
PKA:7.76±0.47(Predicted)
PSA：74.16000
Density:1.251±0.06 g/cm3(Predicted)
LogP:1.41700
XLogP3:-0.2
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:1
Exact Mass:139.074561919
Heavy Atom Count:10
Complexity:109

Purity/Quality:

98%min ^*data from raw suppliers

4-Methoxy-pyridine-2,3-diamine 95% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=C(C(=NC=C1)N)N

Technology Process of 2,3-Diamino-4-methoxypyridine

There total 7 articles about 2,3-Diamino-4-methoxypyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.6%

: 84487-08-1
4-methoxy-3-nitro-pyridin-2-ylamine

: 127356-16-5
4-methoxy-pyridine-2,3-diamine

Guidance literature:: With palladium on activated charcoal; hydrogen; In methanol; at 20 ℃; for 16h;

Reference yield:

: 6980-08-1
4-chloro-3-nitro-2-pyridinamine

: 127356-16-5
4-methoxy-pyridine-2,3-diamine

Guidance literature:: Multi-step reaction with 2 steps

1: 56 percent / Na / 2 h / Heating

2: 87 percent / H₂ / 10percent Pd/C / methanol / 1 h / 760 Torr

With hydrogen; sodium; palladium on activated charcoal; In methanol;
DOI:10.1021/jm00170a030

Reference yield:

: 19798-80-2
2-Amino-4-chloropyridine

: 127356-16-5
4-methoxy-pyridine-2,3-diamine

Guidance literature:: Multi-step reaction with 3 steps

1.1: sulfuric acid; nitric acid / 2 h / 0 - 20 °C

1.2: pH 9

2.1: 16 h / 60 °C

2.2: pH 6

3.1: palladium 10% on activated carbon; hydrogen / methanol / 2 h / 20 °C / 750.08 Torr

With sulfuric acid; palladium 10% on activated carbon; hydrogen; nitric acid; In methanol;