Carbamic acid, (1-methylpropyl)-, 1,1-dimethylethyl ester, (R)- (9CI)

Base Information

Chemical Name:Carbamic acid, (1-methylpropyl)-, 1,1-dimethylethyl ester, (R)- (9CI)
CAS No.:129991-09-9
Molecular Formula:C9H19NO2
Molecular Weight:173.25266
Hs Code.:
Mol file:129991-09-9.mol

Synonyms:Carbamic acid, (1-methylpropyl)-, 1,1-dimethylethyl ester, (R)- (9CI)

Suppliers and Price of Carbamic acid, (1-methylpropyl)-, 1,1-dimethylethyl ester, (R)- (9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
(R)-tert-Butylsec-butylcarbamate 95+%
1g
$ 470.00

Total 1 raw suppliers

Chemical Property of Carbamic acid, (1-methylpropyl)-, 1,1-dimethylethyl ester, (R)- (9CI)

Chemical Property:

Boiling Point:211.4±8.0 °C(Predicted)
PKA:13.06±0.46(Predicted)
PSA：38.33000
Density:0.912±0.06 g/cm3(Predicted)
LogP:2.70050

Purity/Quality:: (R)-tert-Butylsec-butylcarbamate 95+% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Carbamic acid, (1-methylpropyl)-, 1,1-dimethylethyl ester, (R)- (9CI)

There total 1 articles about Carbamic acid, (1-methylpropyl)-, 1,1-dimethylethyl ester, (R)- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 13250-12-9
(R)-sec-butylamine

: 24424-99-5
di-tert-butyl dicarbonate

: 129991-09-9
(R)-N-Boc-2-aminobutane

Guidance literature:: In dichloromethane; for 1h; Ambient temperature;
DOI:10.1016/S0040-4020(01)85630-1

Reference yield:

: 129991-09-9
(R)-N-Boc-2-aminobutane

: 124-63-0
methanesulfonyl chloride

: 126301-16-4,149602-63-1,126301-17-5
(2R)-2-[(tert-butoxycarbonyl)amino]propyl methanesulfonate

Guidance literature:: With triethylamine; In dichloromethane;

Reference yield:

: 129991-09-9
(R)-N-Boc-2-aminobutane

: 454248-53-4
(R)-4-methyl-2,2-dioxo-1,2,3-oxathiazolidine-3-carboxylic acid tert butyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 1H-imidazole; triethylamine; thionyl chloride / dichloromethane / 21 h / -70 - 20 °C / Inert atmosphere

2: ruthenium(III) trichloride hydrate; sodium periodate / acetonitrile; water / 16 h / 11 - 20 °C / Inert atmosphere

With 1H-imidazole; sodium periodate; thionyl chloride; ruthenium(III) trichloride hydrate; triethylamine; In dichloromethane; water; acetonitrile;