2-Pyrrolidinecarboxaldehyde, 1-(2-methyl-2-propenyl)-, (S)- (9CI)

Base Information

Chemical Name:2-Pyrrolidinecarboxaldehyde, 1-(2-methyl-2-propenyl)-, (S)- (9CI)
CAS No.:130823-69-7
Molecular Formula:C9H15NO
Molecular Weight:153.2215
Hs Code.:
Mol file:130823-69-7.mol

Synonyms:2-Pyrrolidinecarboxaldehyde, 1-(2-methyl-2-propenyl)-, (S)- (9CI)

Suppliers and Price of 2-Pyrrolidinecarboxaldehyde, 1-(2-methyl-2-propenyl)-, (S)- (9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 2-Pyrrolidinecarboxaldehyde, 1-(2-methyl-2-propenyl)-, (S)- (9CI)

Chemical Property:

PSA：20.31000
LogP:1.16370

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2-Pyrrolidinecarboxaldehyde, 1-(2-methyl-2-propenyl)-, (S)- (9CI)

There total 3 articles about 2-Pyrrolidinecarboxaldehyde, 1-(2-methyl-2-propenyl)-, (S)- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 130823-72-2
[(S)-1-(2-Methyl-allyl)-pyrrolidin-2-yl]-methanol

: 130823-69-7
(S)-1-(2-Methyl-allyl)-pyrrolidine-2-carbaldehyde

Guidance literature:: With oxalyl dichloride; dimethyl sulfoxide; triethylamine; In dichloromethane; at -78 ℃;
DOI:10.1016/S0040-4039(00)97696-2

Reference yield:

: 33305-75-8,131477-20-8
L-proline ethyl ester monohydrochloride

: 130823-69-7
(S)-1-(2-Methyl-allyl)-pyrrolidine-2-carbaldehyde

Guidance literature:: Multi-step reaction with 3 steps

1: 80 percent / K₂CO₃ / benzene / Heating

2: 79 percent / LiAlH₄ / diethyl ether / Ambient temperature

3: 90 percent / (COCl)2, DMSO, Et₃N / CH₂Cl₂ / -78 °C

With lithium aluminium tetrahydride; oxalyl dichloride; potassium carbonate; dimethyl sulfoxide; triethylamine; In diethyl ether; dichloromethane; benzene;
DOI:10.1016/S0040-4039(00)97696-2

Reference yield:

: 130823-68-6
(S)-1-(2-Methyl-allyl)-pyrrolidine-2-carboxylic acid ethyl ester

: 130823-69-7
(S)-1-(2-Methyl-allyl)-pyrrolidine-2-carbaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1: 79 percent / LiAlH₄ / diethyl ether / Ambient temperature

2: 90 percent / (COCl)2, DMSO, Et₃N / CH₂Cl₂ / -78 °C

With lithium aluminium tetrahydride; oxalyl dichloride; dimethyl sulfoxide; triethylamine; In diethyl ether; dichloromethane;
DOI:10.1016/S0040-4039(00)97696-2