Pyrazino[1,2-d][1,4]diazepine-1,9(2H,6H)-dione, 3,4,7,8-tetrahydro- (9CI)

Base Information

• Chemical Name: Pyrazino[1,2-d][1,4]diazepine-1,9(2H,6H)-dione, 3,4,7,8-tetrahydro- (9CI)
• CAS No.: 130947-34-1
• Molecular Formula: C₈H₁₁N₃O₂
• Molecular Weight: 181.194
• Mol file: 130947-34-1.mol

Synonyms:Pyrazino[1,2-d][1,4]diazepine-1,9(2H,6H)-dione, 3,4,7,8-tetrahydro- (9CI);3,4,7,8-TETRAHYDROPYRAZINO[1,2-D][1,4]DIAZEPINE-1,9(2H,6H)-DIONE

Chemical Property of Pyrazino[1,2-d][1,4]diazepine-1,9(2H,6H)-dione, 3,4,7,8-tetrahydro- (9CI)

Chemical Property:

• PSA: 68.42000
• LogP: -1.07840

Purity/Quality:

99%min ^*data from raw suppliers

3,4,7,8-tetrahydro-Pyrazino[1,2-d][1,4]diazepine-1,9(2H,6H)-dione 97.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Pyrazino[1,2-d][1,4]diazepine-1,9(2H,6H)-dione, 3,4,7,8-tetrahydro- (9CI)

There total 1 articles about Pyrazino[1,2-d][1,4]diazepine-1,9(2H,6H)-dione, 3,4,7,8-tetrahydro- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 22.0%

3-azapentane-1,5-diamine (111-40-0,98824-35-2) + dimethyl acetylenedicarboxylate (762-42-5) → 3,4,7,8-tetrahydro-2H,6H-pyrazino-<1.2-d><1.4>diazepine-1,9-dione (130947-34-1)

Guidance literature:

In ethanol; at 0 ℃; for 5h;

Reference yield: 90.0%

3,4,7,8-tetrahydro-2H,6H-pyrazino-<1.2-d><1.4>diazepine-1,9-dione (130947-34-1) → hexahydropyrazino<1.2-d><1.4>diazepine-1,9-dione (130947-37-4)

Guidance literature:

With hydrogen; palladium dihydroxide; In water; for 12h;

upstream raw materials:

3-azapentane-1,5-diamine

dimethyl acetylenedicarboxylate

Downstream raw materials:

hexahydropyrazino<1.2-d><1.4>diazepine-1,9-dione

Refernces