Benzofuran,2,3-dihydro-7-(1-methylethyl)-(9CI)

Base Information

Chemical Name:Benzofuran,2,3-dihydro-7-(1-methylethyl)-(9CI)
CAS No.:131180-38-6
Molecular Formula:C₁₁H₁₄O
Molecular Weight:162.232
Hs Code.:
Mol file:131180-38-6.mol

Synonyms:Benzofuran,2,3-dihydro-7-(1-methylethyl)-(9CI)

Suppliers and Price of Benzofuran,2,3-dihydro-7-(1-methylethyl)-(9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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Total 1 raw suppliers

Chemical Property of Benzofuran,2,3-dihydro-7-(1-methylethyl)-(9CI)

Chemical Property:

Boiling Point:79 - 81 °C (15 mmHg)
PSA：9.23000
LogP:2.74490

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Benzofuran,2,3-dihydro-7-(1-methylethyl)-(9CI)

There total 5 articles about Benzofuran,2,3-dihydro-7-(1-methylethyl)-(9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 157-18-6
oxirene

: 19099-54-8
2-isopropyliodobenzene

: 131180-38-6
7-isopropyl-2,3-dihydrobenzofuran

Guidance literature:: With palladium diacetate; XPhos; In 1-methyl-pyrrolidin-2-one; at 80 ℃; for 24h; Inert atmosphere; Sealed tube;

Reference yield: 77.0%

: 75-21-8,99932-75-9
oxirane

: 19099-54-8
2-isopropyliodobenzene

: 131180-38-6
7-isopropyl-2,3-dihydrobenzofuran

Guidance literature:: With palladium diacetate; potassium bicyclo[2.2.1]hept-2-ene-5-carboxylate; XPhos; In 1-methyl-pyrrolidin-2-one; at 80 ℃; for 24h;
DOI:10.1055/s-0039-1690779

Reference yield:

: 88-69-7
2-(1-methylethyl)phenol

: 131180-38-6
7-isopropyl-2,3-dihydrobenzofuran

Guidance literature:: Multi-step reaction with 3 steps

1: aq. Br₂-KBr / aq. ethanol / 1 h / Ambient temperature

2: NaOH / H₂O / 6 h / Heating

3: 1) n-BuLi, 2) n-BuLi / 1) THF, cyclohexane, hexane, -100 deg C, 30 min, 2) hexane, -100 deg C, 1h

With sodium hydroxide; n-butyllithium; bromine; potassium bromide; In ethanol; water;
DOI:10.1021/jo00002a026