4,4'-Bipyridyl-d8

Base Information

• Chemical Name: 4,4'-Bipyridyl-d8
• CAS No.: 132125-39-4
• Molecular Formula: C10D8N2
• Molecular Weight: 164.23
• European Community (EC) Number: 808-642-0
• Nikkaji Number: J2.263.766E
• Mol file: 132125-39-4.mol

Synonyms:4,4'-Bipyridyl-d8;132125-39-4;4,4'-DIPYRIDYL-D8;2,3,5,6-tetradeuterio-4-(2,3,5,6-tetradeuteriopyridin-4-yl)pyridine;4,4 inverted exclamation marka-Dipyridyl-d8;HY-W017289S;4,4'-Bipyridyl-d8, 98 atom % D;CS-0564271;D98395

Chemical Property of 4,4'-Bipyridyl-d8

Chemical Property:

• Melting Point: 111-114 °C(lit.)
• PSA: 25.78000
• LogP: 2.14360
• XLogP3: 1.4
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 1
• Exact Mass: 164.118962231
• Heavy Atom Count: 12
• Complexity: 108

Purity/Quality:

99% by CP; 98% atom D ^*data from raw suppliers

4,4''-Dipyridyl-d8 ^*data from reagent suppliers

Safty Information:

• Pictogram(s): T
• Hazard Codes: T
• Statements: 25-36/37/38
• Safety Statements: 26-36/37/39-45

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CN=CC=C1C2=CC=NC=C2
• Isomeric SMILES: [2H]C1=C(N=C(C(=C1C2=C(C(=NC(=C2[2H])[2H])[2H])[2H])[2H])[2H])[2H]

Technology Process of 4,4'-Bipyridyl-d8

There total 1 articles about 4,4'-Bipyridyl-d8 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

4,4'-bipyridine (553-26-4) → 4,4'-bipyridine-d8 (132125-39-4)

Guidance literature:

platinum(IV) oxide; In water-d2; at 250 ℃; for 8h; under 30002.4 Torr;

DOI:10.3987/COM-05-S(T)36

Reference yield:

zinc(II) nitrate hexahydrate + bis(4-carboxyphenyl)sulfone (2449-35-6) + 4,4'-bipyridine-d8 (132125-39-4) → [Zn2(sdb)2(bpy-d8)]

Guidance literature:

In N,N-dimethyl-formamide; at 100 ℃; for 48h; Sealed tube;

DOI:10.1021/ic302006x

Reference yield:

methylene chloride (74-87-3) + 4,4'-bipyridine-d8 (132125-39-4) → methyl viologen dichloride (347841-45-6)

Guidance literature:

In water; at 130 ℃; for 8h;

DOI:10.1039/f19848003257

upstream raw materials:

4,4'-bipyridine

Downstream raw materials:

methyl viologen dichloride

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