Carbamic acid, (1-methyl-2-propenyl)(2-oxoethyl)-, ethyl ester (9CI)

Base Information

Chemical Name:Carbamic acid, (1-methyl-2-propenyl)(2-oxoethyl)-, ethyl ester (9CI)
CAS No.:132414-77-8
Molecular Formula:C9H15NO3
Molecular Weight:185.22
Hs Code.:
Mol file:132414-77-8.mol

Synonyms:Carbamic acid, (1-methyl-2-propenyl)(2-oxoethyl)-, ethyl ester (9CI)

Suppliers and Price of Carbamic acid, (1-methyl-2-propenyl)(2-oxoethyl)-, ethyl ester (9CI)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Carbamic acid, (1-methyl-2-propenyl)(2-oxoethyl)-, ethyl ester (9CI)

Chemical Property:

Boiling Point:242.7±29.0 °C(Predicted)
PKA:-1.83±0.70(Predicted)
PSA：0.00000
Density:1.025±0.06 g/cm3(Predicted)
LogP:0.00000

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

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Technology Process of Carbamic acid, (1-methyl-2-propenyl)(2-oxoethyl)-, ethyl ester (9CI)

There total 4 articles about Carbamic acid, (1-methyl-2-propenyl)(2-oxoethyl)-, ethyl ester (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: ethyl (R)-but-3-en-2-yl(2,2-dimethoxyethyl)carbamate

: 132414-77-8
ethyl (R)-but-3-en-2-yl(2-oxoethyl)carbamate

Guidance literature:: With toluene-4-sulfonic acid; In water; acetone; at 60 ℃; for 18h;

Reference yield: 91.0%

: 132414-76-7
ethyl but-3-en-2-yl-(2,2-dimethoxyethyl)carbamate

: 132414-77-8
ethyl but-3-en-2-yl(2-oxoethyl)carbamate

Guidance literature:: With formic acid; at 0 - 100 ℃; for 2h;

Reference yield:

: 71545-60-3
ethyl N-(2,2-dimethoxyethyl)carbamate

: 132414-77-8
ethyl but-3-en-2-yl(2-oxoethyl)carbamate

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / mineral oil; N,N-dimethyl-formamide / 2 h / 0 °C

1.2: 20 h / 20 °C

2.1: formic acid / 2 h / 0 - 100 °C

With formic acid; sodium hydride; In N,N-dimethyl-formamide; mineral oil;