n'-(3-Chlorobenzylidene)benzohydrazide

Base Information

Chemical Name:n'-(3-Chlorobenzylidene)benzohydrazide
CAS No.:39575-05-8
Molecular Formula:C14H11 Cl N2 O
Molecular Weight:258.707
Hs Code.:
NSC Number:148197
ChEMBL ID:CHEMBL2235153

Synonyms:n'-(3-chlorobenzylidene)benzohydrazide;NSC148197;CHEMBL2235153;SCHEMBL13475714;BDBM192653;39575-05-8;AKOS002965047;NSC-148197;SR-01000198250;SR-01000198250-1;N’-(3-chlorophenylmethylene)benzohydrazide (1d);N'-[(E)-(3-CHLOROPHENYL)METHYLIDENE]BENZOHYDRAZIDE

Suppliers and Price of n'-(3-Chlorobenzylidene)benzohydrazide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of n'-(3-Chlorobenzylidene)benzohydrazide

Chemical Property:

XLogP3:3.2
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:3
Exact Mass:258.0559907
Heavy Atom Count:18
Complexity:300

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)C(=O)NN=CC2=CC(=CC=C2)Cl
Isomeric SMILES:C1=CC=C(C=C1)C(=O)N/N=C/C2=CC(=CC=C2)Cl

Technology Process of n'-(3-Chlorobenzylidene)benzohydrazide

There total 2 articles about n'-(3-Chlorobenzylidene)benzohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.71%

: 613-94-5
benzoic acid hydrazide

: 587-04-2
m-Chlorobenzaldehyde

: 39575-05-8
N’-(3-chlorophenylmethylene)benzohydrazide

Guidance literature:: With acetic acid; In ethanol; Reflux;
DOI:10.1016/j.bioorg.2016.05.003

Reference yield:

: 65-85-0,8013-63-6
benzoic acid

: 39575-05-8
N’-(3-chlorophenylmethylene)benzohydrazide

Guidance literature:: Multi-step reaction with 2 steps

1: hydrazine hydrate monohydrate

2: acetic acid / ethanol / Reflux

With hydrazine hydrate monohydrate; acetic acid; In ethanol;
DOI:10.1016/j.bioorg.2016.05.003

Reference yield: 92.0%

: 39575-05-8
N’-(3-chlorophenylmethylene)benzohydrazide

: 106-95-6
allyl bromide

: 1242159-30-3
(S)-N'-[1-(3-chlorophenyl)but-3-enyl]benzohydrazide

Guidance literature:: N’-(3-chlorophenylmethylene)benzohydrazide; With C₃₄H₃₂N₂O₂*F₆P^(1-)*H⁽¹⁺⁾; In methanol; at 20 ℃; for 1h; Inert atmosphere;

allyl bromide; With indium; In methanol; at 20 ℃; for 12h; Inert atmosphere;

With water; sodium hydrogencarbonate; In methanol; dichloromethane; optical yield given as %ee; enantioselective reaction; Inert atmosphere;
DOI:10.1016/j.tet.2012.06.061