(2,2,6,6-TETRAMETHYL-3,5-HEPTANEDIONATO)THALLIUM(I)

Base Information

Chemical Name:(2,2,6,6-TETRAMETHYL-3,5-HEPTANEDIONATO)THALLIUM(I)
CAS No.:133892-72-5
Molecular Formula:C11H19O2Tl
Molecular Weight:387.65
Hs Code.:
Mol file:133892-72-5.mol

Synonyms:(2,2,6,6-TETRAMETHYL-3,5-HEPTANEDIONATO)THALLIUM(I);TI(TMHD)

Suppliers and Price of (2,2,6,6-TETRAMETHYL-3,5-HEPTANEDIONATO)THALLIUM(I)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Strem Chemicals
2,2,6,6-Tetramethyl-3,5-heptanedionatothallium(I), 99% [Tl(TMHD)] 99% [Tl(TMHD)]
5g
$ 343.00

Strem Chemicals
2,2,6,6-Tetramethyl-3,5-heptanedionatothallium(I), 99% [Tl(TMHD)] 99% [Tl(TMHD)]
1g
$ 87.00

Total 3 raw suppliers

Chemical Property of (2,2,6,6-TETRAMETHYL-3,5-HEPTANEDIONATO)THALLIUM(I)

Chemical Property:

PSA：26.30000
LogP:3.01250

Purity/Quality:

85.0-99.8% ^*data from raw suppliers

2,2,6,6-Tetramethyl-3,5-heptanedionatothallium(I), 99% [Tl(TMHD)] 99% [Tl(TMHD)] ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of (2,2,6,6-TETRAMETHYL-3,5-HEPTANEDIONATO)THALLIUM(I)

There total 2 articles about (2,2,6,6-TETRAMETHYL-3,5-HEPTANEDIONATO)THALLIUM(I) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 1118-71-4
2,2,6,6-tetramethylheptane-3,5-dione

: 20398-06-5
thallium (I) ethoxide

: 133892-72-5
(2,2,6,6-tetramethyl-3,5-heptanedionato)thallium(I) polymer

Guidance literature:: In pentane; byproducts: C2H5OH; inert atm.; to a soln. of dione in n-pentane TiOC2H5 was added, stirred overnight; evapd. to dryness under vac.; elem. anal.;
DOI:10.1016/j.ica.2004.07.053

Reference yield:

: 1118-71-4
2,2,6,6-tetramethylheptane-3,5-dione

: 22537-56-0
thallium(I) ion

: 133892-72-5
(2,2,6,6-tetramethyl-3,5-heptanedionato)thallium(I) polymer

Guidance literature:: With sodium hydroxide; In ethanol; addn. of (CH3)3CCOCH2COC(CH3)3 to an ethanolic Tl(1+) soln.; the pH was adjusted to 9-10 by adding NaOH soln.;; the ppt. was filtered off and dried; sublimation under vac.; elem. anal.;;
DOI:10.1016/S0020-1693(00)82897-2

Reference yield:

: 133892-72-5
(2,2,6,6-tetramethyl-3,5-heptanedionato)thallium(I) polymer

: 75-71-8
Dichlorodifluoromethane

: 55172-29-7,7791-12-0
thallium chloride

Guidance literature:: In neat (no solvent); the Tl complex was heated at 180°C in the vaporization zone and the chemical vapor deposition was initiated in the reaction zone at 450°C using CF2Cl2/O2 gas mixture;;
DOI:10.1016/S0020-1693(00)82897-2