phenyl phenylmethanesulfonate

Base Information

Chemical Name:phenyl phenylmethanesulfonate
CAS No.:10271-81-5
Molecular Formula:C13H12 O3 S
Molecular Weight:248.302
Hs Code.:

Synonyms:a-Toluenesulfonic acid, phenylester (7CI,8CI); NSC 254053; Phenyl benzylsulfonate; Phenylphenylmethanesulfonate; Phenyl toluene-a-sulfonate

Suppliers and Price of phenyl phenylmethanesulfonate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 6 raw suppliers

Chemical Property of phenyl phenylmethanesulfonate

Chemical Property:

Vapor Pressure:1.64E-06mmHg at 25°C
Boiling Point:408.6°C at 760 mmHg
Flash Point:200.9°C
Density:1.272g/cm³

Purity/Quality:: 98%min ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of phenyl phenylmethanesulfonate

There total 4 articles about phenyl phenylmethanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 108-95-2,27073-41-2
phenol

: 1939-99-7
benzenesulfonyl chloride

: 10271-81-5
phenyl toluene-α-sulphonate

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; for 1.83333h;
DOI:10.1002/ejoc.201701766

Reference yield:

: 100-44-7
benzyl chloride

: 10271-81-5
phenyl toluene-α-sulphonate

Guidance literature:: Multi-step reaction with 2 steps

1.1: thiourea; ethanol / 3 h / 96 °C / Inert atmosphere; Sealed tube

1.2: 0.25 h / 0 °C / Inert atmosphere; Sealed tube

1.3: 0.5 h / 20 °C / Inert atmosphere; Sealed tube

2.1: sodium hydride / tetrahydrofuran; mineral oil / 0.17 h / Inert atmosphere; Sealed tube

2.2: 20 °C / Inert atmosphere; Sealed tube

With ethanol; sodium hydride; thiourea; In tetrahydrofuran; mineral oil;
DOI:10.1002/anie.201503112