o-Tolualdehyde-13C1 (carbonyl-13C)

Base Information

Chemical Name:o-Tolualdehyde-13C1 (carbonyl-13C)
CAS No.:138151-99-2
Molecular Formula:CH3C6H413CHO
Molecular Weight:121.14
Hs Code.:

Synonyms:[carbaldehyde-13C]-o-tolualdehyde;[carbonyl-13C] o-tolualdehyde;2-methyl-[α-13C]benzaldehyde;o-Methyl-benzaldehyd-7-13C;

Suppliers and Price of o-Tolualdehyde-13C1 (carbonyl-13C)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Medical Isotopes, Inc.
o-Tolualdehyde-13C1(carbonyl-13C)
0.5 g
$ 860.00

Total 2 raw suppliers

Chemical Property of o-Tolualdehyde-13C1 (carbonyl-13C)

Chemical Property:

PSA：17.07000
LogP:1.80750

Purity/Quality:

97% ^*data from raw suppliers

o-Tolualdehyde-13C1(carbonyl-13C) ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Uses o-Tolualdehyde-13C1 (carbonyl-13C) (CAS# 138151-99-2) is a useful isotopically labeled research compound.

Technology Process of o-Tolualdehyde-13C1 (carbonyl-13C)

There total 6 articles about o-Tolualdehyde-13C1 (carbonyl-13C) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 339222-04-7
o-methyl<α-13C>benzyl alcohol

: 138151-99-2
2-methylbenzaldehyde

Guidance literature:: With ammonium cerium(IV) nitrate; In water; at 40 - 50 ℃;
DOI:10.1021/ja00236a038

Reference yield: 76.0%

: 10383-90-1
⁽¹³⁾C-benzaldehyde

: 74-88-4
methyl iodide

: 138151-99-2
2-methylbenzaldehyde

Guidance literature:: ⁽¹³⁾C-benzaldehyde; With n-butyllithium; N,N',N'-trimethylenediamine; In tetrahydrofuran; at -20 ℃; for 14h; Inert atmosphere; Schlenk technique; Glovebox;

methyl iodide; at -40 - 20 ℃; for 0.5h;
DOI:10.1021/ja504892c

Reference yield:

: 136391-75-8
methyl -o-toluate

: 138151-99-2
2-methylbenzaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / LiAlH₄ / tetrahydrofuran / Heating

2: 75 percent / pyridinium chlorochromate / CH₂Cl₂ / 4 h / 20 °C

With lithium aluminium tetrahydride; pyridinium chlorochromate; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ja0039482