3-Pyridinecarboxaldehyde, 1,4-dihydro-2,6-dimethyl-4-oxo- (9CI)

Base Information

Chemical Name:3-Pyridinecarboxaldehyde, 1,4-dihydro-2,6-dimethyl-4-oxo- (9CI)
CAS No.:138642-53-2
Molecular Formula:C₈H₉NO₂
Molecular Weight:151.165
Hs Code.:
Mol file:138642-53-2.mol

Synonyms:3-Pyridinecarboxaldehyde, 1,4-dihydro-2,6-dimethyl-4-oxo- (9CI)

Suppliers and Price of 3-Pyridinecarboxaldehyde, 1,4-dihydro-2,6-dimethyl-4-oxo- (9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of 3-Pyridinecarboxaldehyde, 1,4-dihydro-2,6-dimethyl-4-oxo- (9CI)

Chemical Property:

PSA：49.93000
LogP:0.80420

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 3-Pyridinecarboxaldehyde, 1,4-dihydro-2,6-dimethyl-4-oxo- (9CI)

There total 2 articles about 3-Pyridinecarboxaldehyde, 1,4-dihydro-2,6-dimethyl-4-oxo- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 28.0%

: 7516-31-6
2,6-dimethyl-1H-pyridin-4-one

: 67-66-3,8013-54-5
chloroform

: 138642-53-2
2,6-dimethyl-3-formyl-4(1H)-pyridone

Guidance literature:: With sodium hydroxide; for 6h; Heating;
DOI:10.1021/jm00061a016

Reference yield:

: 7516-31-6
2,6-dimethyl-1H-pyridin-4-one

: 138642-53-2
2,6-dimethyl-3-formyl-4(1H)-pyridone

Guidance literature:: In sodium hydroxide; chloroform;

Reference yield:

: 138642-53-2
2,6-dimethyl-3-formyl-4(1H)-pyridone

: 2,6-Dimethyl-4-[2'-(1H-tetrazol-5-yl)-biphenyl-4-ylmethoxy]-pyridine-3-carbaldehyde; hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) NaH / 1.) DMF, 2.) DMF, 40 deg C, 1.5 h

2: conc. HCl / ethanol; methanol / 2 h

With hydrogenchloride; sodium hydride; In methanol; ethanol;
DOI:10.1021/jm00061a016