1,1-Dichloro-4,4-dimethylpent-2-yne

Base Information

Chemical Name:1,1-Dichloro-4,4-dimethylpent-2-yne
CAS No.:139185-47-0
Molecular Formula:C7H10Cl2
Molecular Weight:0
Hs Code.:
Mol file:139185-47-0.mol

Synonyms:1,1-Dichloro-4,4-dimethylpent-2-yne

Suppliers and Price of 1,1-Dichloro-4,4-dimethylpent-2-yne

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 1 raw suppliers

Chemical Property of 1,1-Dichloro-4,4-dimethylpent-2-yne

Chemical Property:

PSA：0.00000
LogP:2.83960

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 1,1-Dichloro-4,4-dimethylpent-2-yne

There total 4 articles about 1,1-Dichloro-4,4-dimethylpent-2-yne which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 999-78-0
4,4-dimethyl-2-pentyne

: 139185-47-0
1,1-dichloro-4,4-dimethylpent-2-yne

Guidance literature:: 4,4-dimethyl-2-pentyne; With n-butyllithium; In diethyl ether; N,N-dimethyl-formamide; at -40 - 20 ℃; for 0.5h; Inert atmosphere;

With phosphorus pentachloride; In dichloromethane; at -20 ℃; Inert atmosphere;
DOI:10.1021/ol302790e

Reference yield:

: 2579-21-7
4,4-dimethylpent-2-ynal

: 139185-47-0
1,1-dichloro-4,4-dimethylpent-2-yne

Guidance literature:: With pyridine; phosphorus pentachloride; In dichloromethane; at -20 ℃; for 0.333333h; Yield given;
DOI:10.1007/BF00864534

Reference yield:

: 52323-98-5
4,4-dimethylpent-2-yn-1-ol

: 139185-47-0
1,1-dichloro-4,4-dimethylpent-2-yne

Guidance literature:: With pyridine; CrO₃*pyridinium hydrochloride; phosphorus pentachloride; Yield given. Multistep reaction; 1) CH₂Cl₂, 15-20 deg C, 2.5 h, 2) -20 deg C, 20-30 min;